Use of Reversed-Phase HPLC for the Qualitative and Quantitative Control of the Production of N-Octadecyl-1,3-Diaminopropane
- 作者: Soldatov M.1, Nosova V.1, Monin E.1, Storozhenko P.1
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隶属关系:
- State Research Institute for Chemistry and Technology of Organoelement Compounds
- 期: 卷 74, 编号 2 (2019)
- 页面: 121-125
- 栏目: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/183142
- DOI: https://doi.org/10.1134/S1061934818120080
- ID: 183142
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详细
Using reversed-phase HPLC, we developed a procedure for the qualitative and quantitative analytical control of the production of N-octadecyl-1,3-diaminopropane from stearic acid by the nitrile method. The optimum composition of the eluent is determined, which ensures the control of each stage of the process. The calibration dependences for the mixtures initial reagent–reaction product are obtained, suggesting a quantitative estimation of the conversion. The possibility of determining the presence of synthesis by products is shown. The analysis time for each stage does not exceed 20 min.
作者简介
M. Soldatov
State Research Institute for Chemistry and Technology of Organoelement Compounds
编辑信件的主要联系方式.
Email: soldat89.89@gmail.com
俄罗斯联邦, Moscow, 105118
V. Nosova
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: soldat89.89@gmail.com
俄罗斯联邦, Moscow, 105118
E. Monin
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: soldat89.89@gmail.com
俄罗斯联邦, Moscow, 105118
P. Storozhenko
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: soldat89.89@gmail.com
俄罗斯联邦, Moscow, 105118
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