Determination of selenium and cadmium dopants in nanocomposites based on zinc and indium oxides by high resolution continuous source electrothermal atomic absorption spectrometry and inductively coupled plasma mass spectrometry


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An approach is proposed to the determination of selenium and cadmium dopants in new nanocomposites based on zinc and indium oxides. The approach is based on a combination of highly efficient high resolution continuous source electrothermal atomic absorption spectrometry (ETAAS) for the analysis of suspensions and inductively coupled plasma mass spectrometry for the analysis of solutions. A procedure is developed for the determination of Se and Cd dopants and matrix components based on Zn and In in nanocomposite solutions by inductively coupled plasma mass spectrometry. Stabilizing agents for the preparation of suspensions are studied for the ETAAS analysis of powders without their decomposition. The results of determination of CdSe dopants by high resolution ETAAS are validated by inductively coupled plasma mass spectrometry.

作者简介

D. Filatova

Department of Chemistry; Giredmet Scientific-Research and Design Institute of Rare-Metal Industry

编辑信件的主要联系方式.
Email: gak1.analyt@gmail.com
俄罗斯联邦, Moscow, 119991; Bol’shoi Tolmachevskii per. 5, building 1, Moscow, 119017

V. Es’kina

MISiS National University of Science and Technology

Email: gak1.analyt@gmail.com
俄罗斯联邦, Leninskii pr. 4, Moscow, 119049

A. Chizhov

Department of Chemistry

Email: gak1.analyt@gmail.com
俄罗斯联邦, Moscow, 119991

M. Rumyantseva

Department of Chemistry

Email: gak1.analyt@gmail.com
俄罗斯联邦, Moscow, 119991

P. Shaposhnik

Department of Chemistry

Email: gak1.analyt@gmail.com
俄罗斯联邦, Moscow, 119991

V. Baranovskaya

Giredmet Scientific-Research and Design Institute of Rare-Metal Industry; MISiS National University of Science and Technology

Email: gak1.analyt@gmail.com
俄罗斯联邦, Bol’shoi Tolmachevskii per. 5, building 1, Moscow, 119017; Leninskii pr. 4, Moscow, 119049

Yu. Karpov

Kurnakov Institute of General and Inorganic Chemistry

Email: gak1.analyt@gmail.com
俄罗斯联邦, Leninskii pr. 31, Moscow, 119991


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