Determination of ametoctradin in plant residues and environmental samples by HPLC with an UV detector
- Авторы: Komarova A.1, Chermenskaya T.2, Chelovechkova V.2
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Учреждения:
- OOO Innovation Center for Plant Protection
- All-Russian Scientific Research Institute of Plant Protection
- Выпуск: Том 72, № 10 (2017)
- Страницы: 1076-1081
- Раздел: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/182650
- DOI: https://doi.org/10.1134/S1061934817100082
- ID: 182650
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Аннотация
The study deals with the development of a method for the determination of ametoctradin by HPLC with UV detection. Samples were extracted with aqueous acetone and then purified by distribution between immiscible solvents and also on solid-phase extraction cartridges. The procedure was tested in the determination of ametoctradin in water in the range 0.001–0.01 mg/L, in soil, potato vine and potato tubers, salad, onion, cucumber, tomatoes, carrots, grapes, and grape juice in the range from 0.005 to 0.1 mg/kg, depending on the matrix. The average recoveries were 78−92% with RSD < 0.08%. The proposed procedure is applicable to the determination of ametoctradin in environmental samples and plant residues.
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Об авторах
A. Komarova
OOO Innovation Center for Plant Protection
Email: tchermenskaya@yandex.ru
Россия, St. Petersburg−Pushkin, 196607
T. Chermenskaya
All-Russian Scientific Research Institute of Plant Protection
Автор, ответственный за переписку.
Email: tchermenskaya@yandex.ru
Россия, St. Petersburg−Pushkin, 196608
V. Chelovechkova
All-Russian Scientific Research Institute of Plant Protection
Email: tchermenskaya@yandex.ru
Россия, St. Petersburg−Pushkin, 196608