Problems and optimization of sampling, storage, and sample preparation in the determination of the trace element composition of human saliva


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Abstract

Experimental results are reported on the effect of the procedure of sampling, storage conditions, and sample preparation of saliva on the concentrations of trace elements determined by atomic emission digital spectrography of liquid samples with spectrum excitation from their dry residues in an AC arc at a tip of a carbon electrode. Recommendations on the optimization of the stages of sampling, storage, and preparation of saliva samples are given.

About the authors

S. S. Savinov

Institute of Chemistry

Author for correspondence.
Email: s.s.savinov@spbu.ru
Russian Federation, Universitetskaya nab. 7/9, St. Petersburg, 199034

A. A. Anisimov

Institute of Chemistry

Email: s.s.savinov@spbu.ru
Russian Federation, Universitetskaya nab. 7/9, St. Petersburg, 199034

A. I. Drobyshev

Institute of Chemistry

Email: s.s.savinov@spbu.ru
Russian Federation, Universitetskaya nab. 7/9, St. Petersburg, 199034


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