In situ High-Temperature Synchrotron X-Ray Studies of Microstructure And Phase Composition of Additively Fabricated Ti–6Al–4V/TiC Metal Matrix Composite

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Abstract

The microstructure and phase composition of Ti–6Al–4V/TiC metal matrix composite samples obtained by wire-feed electron-beam additive manufacturing are investigated by X-ray diffraction analysis, optical, scanning and transmission electron microscopy. It is shown that the microstructure of the Ti–6Al–4V/TiC composite consists of primary β-grains containing α/α′-plates separated by interlayers of residual β- and α′′-phases. Irregularly shaped TiC carbide particles with sizes of 1–2 μm are distributed along the boundaries of the primary β-grains. The changes in the phase composition of the 3D-printed Ti–6Al–4V/TiC composites during heating from room temperature to 1100°C are investigated by X-ray diffraction using synchrotron radiation. The changes in the shape and position of the X-ray peaks of α/α′- and β-phases during heating and cooling are analyzed. It is shown that in the temperature range 700–800°C, there is a shift of the 110 peak of the β-phase towards large angles, as well as a change in its full width at half maximum associated with the formation and subsequent decomposition of the orthorhombic α′′-phase.

About the authors

A. V Panin

Institute of Strength Physics and Materials Science SB RAS; National Research Tomsk Polytechnic University

Email: pav@ispms.ru
Tomsk, Russia; Tomsk, Russia

M. S Syrtanov

National Research Tomsk Polytechnic University

Tomsk, Russia

T. A Lobova

Institute of Strength Physics and Materials Science SB RAS

Tomsk, Russia

O. B Perevalova

Institute of Strength Physics and Materials Science SB RAS

Tomsk, Russia

M. S Kazachenok

Institute of Strength Physics and Materials Science SB RAS

Tomsk, Russia

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