Effect of migration of nickel of carbon nanofiber support into active phase of molibdenum disulfide based catalyst of alcohol synthesis

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Abstract

Fibrous carbon produced by catalitic decomposition of methane and containing minor amount of Ni was tested as a support for molybdenum disulfide-based catalysts for reductive conversion of CO into alcohols. It was established for the first time using method of X-ray difraction, transmission and scanning microscopy that during sulfidation of catalyst precursor nickel, incapsulated in carbon, intgrates into layered molybdenum disulfide cristallites, becoming part of the catalytically active Ni–(Co)–Mo–S phase.

About the authors

M. E. Osman

N.D. Zelinsky Institute of Organic Chemistry RAS

Email: osman@ioc.ac.ru
Leninsky Prosp., 47, Moscow, 119991 Russia

E. A. Permyakov

N.D. Zelinsky Institute of Organic Chemistry RAS

Email: permeakra@ioc.ac.ru
Leninsky Prosp., 47, Moscow, 119991 Russia

N. A. Repyov

N.D. Zelinsky Institute of Organic Chemistry RAS; Department of Chemistry, Lomonosov Moscow State University

Leninsky Prosp., 47, Moscow, 119991 Russia; Leninskie gory 1/3, Moscow, 119991 Russia

V. V. Maximov

N.D. Zelinsky Institute of Organic Chemistry RAS

Leninsky Prosp., 47, Moscow, 119991 Russia

V. M. Kogan

N.D. Zelinsky Institute of Organic Chemistry RAS

Leninsky Prosp., 47, Moscow, 119991 Russia

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