Microwave vs Autoclave Synthesis of Nanodisperse ZrN Powder


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Abstract

The synthesis of nanodisperse powers of zirconium nitride ZrN was studied using exothermal reactions initiated by microwave radiation. The obtained ZrN powders were investigated by x-ray phase analysis and scanning electron microscopy. The results showed that nanodisperse materials can be synthesized by means of exothermal reactions upon heating by microwave radiation.

About the authors

R. A. Shishkin

El’tsin Ural Federal University

Author for correspondence.
Email: r.shishkin@yahoo.com
Russian Federation, Ekaterinburg

E. S. Maiorova

El’tsin Ural Federal University

Email: r.shishkin@yahoo.com
Russian Federation, Ekaterinburg

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