Исследование возможности переноса насыщения в новом комплексе никеля(II) с 2,6-бис(пиразол-3-ил)пиридином
- Authors: Aleshin D.Y.1, Nikovskii I.A.1, Khakina E.A.1,2, Danshina A.A.1,3, Nelyubina Y.V.1,4
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Affiliations:
- Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russia
- Russia National Research University Higher School of Economics Moscow, Russia
- Moscow Institute of Physics and Technology (National Research University), Dolgoprudnyi, Moscow oblast, Russia
- Bauman State Technical University, Moscow, Russia
- Issue: Vol 49, No 12 (2023)
- Pages: 737-743
- Section: Articles
- URL: https://journals.rcsi.science/0132-344X/article/view/162365
- DOI: https://doi.org/10.31857/S0132344X22600552
- EDN: https://elibrary.ru/FIJWIJ
- ID: 162365
Cite item
Abstract
By reacting the N,N'-disubstituted 2,6-bis(pyrazol-3-yl)pyridine ligand (L) with a divalent nickel salt, a new nickel(II) complex [Ni(L)(H2O)(THF)Cl]BPh4 was obtained (I), which was isolated in individual form and characterized by elemental analysis, mass spectrometry, NMR spectroscopy and X-ray diffraction (CCDC No. 2221412). According to NMR spectroscopy data in combination with the results of quantum chemical calculations, complex I in solution does not exhibit a saturation transfer effect.
About the authors
D. Yu. Aleshin
Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russia
Email: unelya@ineos.ac.ru
Россия, Москва
I. A. Nikovskii
Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russia
Email: unelya@ineos.ac.ru
Россия, Москва
E. A. Khakina
Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russia; Russia National Research University Higher School of Economics Moscow, Russia
Email: unelya@ineos.ac.ru
Россия, Москва; Россия, Москва
A. A. Danshina
Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russia; Moscow Institute of Physics and Technology (National Research University), Dolgoprudnyi, Moscow oblast, Russia
Email: unelya@ineos.ac.ru
Россия, Москва; Россия, Долгопрудный
Yu. V. Nelyubina
Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russia; Bauman State Technical University, Moscow, Russia
Author for correspondence.
Email: unelya@ineos.ac.ru
Россия, Москва; Россия, Москва
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