Email this article Development of a Sample-Preparation Procedure for Quantitative Determination of Lead in Sugars by Inductively Coupled-Plasma—Atomic-Emission Spectrometry (ICP-AES)
- Authors: Olefir Y.V.1, Sakanyan E.I.1, Ladygina L.A.1, Shchukin V.M.1
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Affiliations:
- Scientific Center for Expert Evaluation of Medicinal Products, Ministry of Health of the Russian Federation
- Issue: Vol 52, No 2 (2018)
- Pages: 171-174
- Section: Article
- URL: https://journals.rcsi.science/0091-150X/article/view/245056
- DOI: https://doi.org/10.1007/s11094-018-1785-6
- ID: 245056
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Abstract
A sample-preparation procedure for the determination of lead in sugars by inductively coupled-plasma—atomic-emission spectrometry was developed and validated using glucose and sucrose as examples. The characteristic detection wavelength and sugar decomposition conditions were selected. The suitability was assessed using a validation protocol for specificity, calibration curve linearity, limits of detection and quantitation, accuracy, precision, and intralaboratory precision.
About the authors
Yu. V. Olefir
Scientific Center for Expert Evaluation of Medicinal Products, Ministry of Health of the Russian Federation
Email: Liana.alex@mail.ru
Russian Federation, 8/2 Petrovskii Blvd., Moscow, 127051
E. I. Sakanyan
Scientific Center for Expert Evaluation of Medicinal Products, Ministry of Health of the Russian Federation
Email: Liana.alex@mail.ru
Russian Federation, 8/2 Petrovskii Blvd., Moscow, 127051
L. A. Ladygina
Scientific Center for Expert Evaluation of Medicinal Products, Ministry of Health of the Russian Federation
Author for correspondence.
Email: Liana.alex@mail.ru
Russian Federation, 8/2 Petrovskii Blvd., Moscow, 127051
V. M. Shchukin
Scientific Center for Expert Evaluation of Medicinal Products, Ministry of Health of the Russian Federation
Email: Liana.alex@mail.ru
Russian Federation, 8/2 Petrovskii Blvd., Moscow, 127051
