Study of the Structure and Properties of Magnetic Nanopowders of Magnetite-Maggemite Series Solid Solutions by SAPNS
- 作者: Shilova O.1, Kovalenko A.1, Nikolaev A.1, Khamova T.1, Kruchinina I.1, Kopitsa G.1,2
-
隶属关系:
- Institute of Silicate Chemistry of Russian Academy of Sciences
- Petersburg Nuclear Physics Institute named by B.P. Konstantinov of the Kurchatov Institute
- 期: 卷 69, 编号 3 (2024)
- 页面: 350-363
- 栏目: STRUCTURE, MAGNETIC AND OPTICAL PROPERTIES OF MATERIALS
- URL: https://journals.rcsi.science/0044-457X/article/view/262879
- DOI: https://doi.org/10.31857/S0044457X24030096
- EDN: https://elibrary.ru/YDZPDI
- ID: 262879
如何引用文章
详细
Nanopowders of the magnetite-maggemite series were synthesized by both aqueous precipitation and using sol-gel technology. A comprehensive comparative study of the structure of the synthesized powders was carried out using the methods of X-ray phase analysis (XPA), scanning electron microscopy (SEM), low-temperature nitrogen adsorption and small-angle polarized neutron scattering (SAPNS). It has been established that the synthesized iron oxide nanopowders are porous systems that, depending on the synthesis method, have a one-level or two-level (for powders obtained by aqueous synthesis) and three-level (for powders obtained by the sol-gel method) hierarchical structure organization with different characteristic scales and types of aggregation for each from structural levels, and the characteristic size for the larger level in both cases exceeds 45 nm. It was revealed that the magnetic structure of the obtained iron oxide powders, regardless of the synthesis method, consists of superparamagnetic particles with a characteristic magnetic radius RМ ≈ 4 nm and magnetic-nuclear cross-correlations RMN ≈ 3 nm for powders obtained by the sol-gel method; and with RM ≈ 5–11 nm and RMN ≈ 4–8 nm for powders obtained by aqueous synthesis, depending on the production conditions.
作者简介
O. Shilova
Institute of Silicate Chemistry of Russian Academy of Sciences
编辑信件的主要联系方式.
Email: olgashilova@bk.ru
俄罗斯联邦, Saint Petersburg
A. Kovalenko
Institute of Silicate Chemistry of Russian Academy of Sciences
Email: olgashilova@bk.ru
俄罗斯联邦, Saint Petersburg
A. Nikolaev
Institute of Silicate Chemistry of Russian Academy of Sciences
Email: olgashilova@bk.ru
俄罗斯联邦, Saint Petersburg
T. Khamova
Institute of Silicate Chemistry of Russian Academy of Sciences
Email: olgashilova@bk.ru
俄罗斯联邦, Saint Petersburg
I. Kruchinina
Institute of Silicate Chemistry of Russian Academy of Sciences
Email: olgashilova@bk.ru
俄罗斯联邦, Saint Petersburg
G. Kopitsa
Institute of Silicate Chemistry of Russian Academy of Sciences; Petersburg Nuclear Physics Institute named by B.P. Konstantinov of the Kurchatov Institute
Email: olgashilova@bk.ru
俄罗斯联邦, Saint Petersburg; Gatchina
参考
- Ferreira M.I., Cova T., Paixão J.A. et al. // Woodhead Publishing Series in Electronic and Optical Materials. Magnetic Nanoparticle-Based Hybrid Materials. Woodhead Publ, 2021. P. 273. https://doi.org/10.1016/B978-0-12-823688-8.00033-8
- Imran M., Shaik A.H., Ansari A.R. et al. // RSC Adv. 2018. V. 8. № 25. P. 13970. https://doi.org/10.1039/C7RA13467C
- Rashid H., Mansoor M.A., Haider B. et al. // Sep. Sci. Technol. 2020. V. 55. № 6. P. 1207. https://doi.org/10.1080/01496395.2019.1585876
- Aphesteguy J.C., Kurlyandskaya G.V., Celis J.P. et al. // Mater. Chem. Phys. 2015. V. 161. Р. 243. https://doi.org/10.1016/j.matchemphys.2015.05.044
- Nazari M., Ghasemi N., Maddah H. et al. // J. Nanostruct. Chem. 2014. V. 4. № 2. P. 99. https://doi.org/10.1007/s40097-014-0099-9
- Ramos Guivar J.A., Martínez A.I., Anaya A.O. et al. // Adv. Nanopart. 2014. V. 3. № 3. P. 114. https://doi.org/10.4236/anp.2014.33016
- Fedorenko N.Yu., Abiev R.Sh., Kudryashova Yu.S. et al. // Ceram. Int. 2022. V. 48. № 9. P. 13006. https://doi.org/10.1016/j.ceramint.2022.01.174
- Шилова О.А., Николаев А.М., Коваленко А.С. и др. // Журн. неорган. химии. 2020. Т. 65. № 3. С. 398.
- Коваленко А.С., Шилова О.А., Николаев А.М. и др. // Коллоид. журнал. 2023. Т. 85. № 3. С. 319.
- Gopinath S., Philip J. // Mater. Chem. Phys. 2014. V. 145. № 1–2. P. 213. https://doi.org/10.1016/j.matchemphys.2014.02.005
- Zienkiewicz-Strzałka M., Skibińska M., Pikus S. // Nucl. Instrum. Methods., Sect. B. 2017. V. 411. P. 72. https://doi.org/10.1016/j.nimb.2017.03.028
- Nirschl H., Guo X. // Chem. Eng. Res. Des. 2018. V. 136. P. 431. https://doi.org/10.1016/j.cherd.2018.06.012
- Shilova O.A., Nikolaev A.M., Kovalenko A.S. et al. // Ceram. Int. 2021. V. 47. № 20. P. 28866. https://doi.org/10.1016/j.ceramint.2021.07.047
- Khamova T.V., Kopitsa G.P., Nikolaev A.M. et al. // Biointer. Res. Appl. Chem. 2021. V. 11. № 4. P. 12285. https://doi.org/10.33263/BRIAC114.1228512300
- Danks A.E., Hall S.R., Schnepp Z. // Mater. Horiz. 2016. V. 3. № 2. P. 91. https://doi.org/10.1039/c5mh00260e
- Okorokov A.I., Runov V.V. // Physica B. 2001. V. 297. № 1–4. P. 239. https://doi.org/10.1016/S0921-4526(00)00843-7
- Fitzsimmons M.R., Schuller I.K. // J. Magn. Magn. Mater. 2014. V. 350. P. 199. https://doi.org/10.1016/j.jmmm.2013.09.028
- Muhlbauer S., Honecker D., P´erigo E.A. et al. // Rev. Mod. Phys. 2019. V. 91. № 1. P. 015004. https://doi.org/10.1103/RevModPhys.91.015004
- Honecker D., Bersweiler M., Erokhin S. et al. // Nanoscale Adv. 2022. V. 4. № 4. P. 1026. https://doi.org/10.1039/D1NA00482D
- Lee S.H., Lee D.H., Jung H. et al. // Curr. Appl. Phys. 2015. V. 15. № 8. P. 915. https://doi.org/10.1016/j.cap.2015.04.003
- Bergenti I., Deriu A., Savini L. et al. // J. Magn. Magn. Mater. 2003. V. 262. № 1. P. 60. https://doi.org/10.1016/S0304-8853(03)00019-2
- Grigoriev S.V., Maleyev S.V., Okorokov A.I. et al. // Europhys. Lett. 2003. V. 63. № 1. Р. 56. https://doi.org/10.1209/epl/i2003-00477-3
- Khamova T.V., Shilova O.A., Gorshkova Yu.E. et al. // Nanosystems: Phys. Chem. Math. 2022. V. 13. № 4. P. 414. https://doi.org/10.17586/2220-8054-2022-13-4-414-429
- Рунов В.В., Бугров А.Н., Смыслов Р.Ю. и др. // Журн. неорган. химии. 2021. Т. 66. № 2. С. 229.
- Fu Z., Xiao Y., Feoktystov A. et al. // Nanoscale. 2016. V. 8. № 43. P. 18541. https://doi.org/10.1039/c6nr06275j
- Zákutná D., Nižňanský D., Barnsley L.C. et al. // Phys. Rev. X. 2020. V. 10. № 3. P. 031019. https://doi.org/10.1103/PhysRevX.10.031019
- Köhler T., Feoktystov A., Petracic O. et al. // Nanoscale. 2021. V. 13. № 4. P. 6965. https://doi.org/10.1039/d0nr08615k
- Chouhan R.S., Horvat M., Ahmed J. et al. // Cancers. 2021. V. 13. № 9. Р. 2213. https://doi.org/10.3390/cancers13092213
- Tran H.-V., Ngo N.M., Medhi R. et al. // Materials. 2022. V. 15. № 2. P. 503. https://doi.org/10.3390/ma15020503
- Kovalenko A.S., Nikolaev A.M., Khamova T.V. et al. // Glass Phys. Chem. 2021. V. 47. № 1. Р. 67. https://doi.org/10.1134/S1087659621070063
- Shilova O.A., Panova G.G., Nikolaev A.M. et al. // Lett. Appl. NanoBioScience. 2021. V. 10. № 2. P. 2215. https://doi.org/10.33263/LIANBS102.22152239
- Wang Y., Wang S., Xu M. et al. // Environ. Pollut. 2019. V. 249. P. 1011. https://doi.org/10.1016/j.envpol.2019.03.119
- Serpoush M., Kiyasatfar M., Ojaghi J. // Mater. Today: Proc. 2022. V. 65. Part 6. P. 2915. https://doi.org/10.1016/j.matpr.2022.06.441
- Turrina Ch., Klassen A., Milani D. et al. // Heliyon. 2023. V. 9. № 6. Р. e16487. https://doi.org/10.1016/j.heliyon.2023.e16487
- Baabu P.R.S., Kumar H.K., Gumpu M.B. et al. // Materials. 2023. V. 16. № 1. P. 59. https://doi.org/10.3390/ma16010059
- Ibarra J., Melendres J., Almada M. et al. // Mater. Res. Exp. 2015. V. 2. № 9. Р. 095010. https://doi.org/10.1088/2053-1591/2/9/095010
- Nasrazadani S., Raman A. // Corros. Sci. 1993. V. 34. № 8. P. 1355. https://doi.org/10.1016/0010-938X(93)90092-U
- Pecharroman C., Gonzalez-Carreno T., Iglesias J.E. // Phys. Chem. Miner. 1995. V. 22. P. 21. https://doi.org/10.1007/BF00202677
- Anthony J.W., Bideaux R.A., Bladh K.W. Magnetite. Handbook of mineralogy. Chantilly, VA: Mineralogical Society of America, 2018.
- Jülich Centre for Neutron Science, QtiKWS 2019. Available online: www.qtisas.com
- Жерновой А.И., Дьяченко С.В. // Журн. техн. физики. 2015. Т. 85. № 4. С. 118.
- Schaefer D.W., Justice R.S. // Macromolecules. 2007. V. 40. № 24. P. 8501. https://doi.org/10.1021/ma070356w
- Баранчиков А.Е., Копица Г.П., Ёров Х.Э. и др. // Журн. неорган. химии. 2021. Т. 66. № 6. С. 774.
- Koizumi S., Yue Z., Tomita Y. et al. // Eur. Phys. J. E. 2008. V. 26. № 1–2. P. 137. https://doi.org/10.1140/epje/i2007-10259-3
- Guinier A., Fournet G., Walker C.B., Yudowitch K.L. Small-Angle Scattering of X-rays. New York: Wiley, 1955.
- Beaucage G., Ulibarri T.A., Black E.P. et al. Hybrid Organic-Inorganic Composites / Eds. By Mark J. et al. ACS Symposium Series; American Chemical Society: Washington, DC, 1995.
- Štěpánek M., Matějíček P., Procházka K. et al. // Langmuir. 2011. V. 27. № 9. P. 5275. https://doi.org/10.1021/la200442s
- Bale H.D., Schmidt P.W. // Phys. Rev. Lett. 1984. V. 53. № 6. P. 596. https://doi.org/10.1103/PhysRevLett.53.596
- Beaucage G. // J. Appl. Crystallogr. 1995. V. 28. № 6. P. 717. https://doi.org/10.1107/S0021889895005292
- Ivanova L.A., Ustinovich K.B., Khamova T.V. et al. // Materials. 2020. V. 13. № 9. P. 2087. https://doi.org/10.3390/ma13092087
- Larsson P.T., Stevanic-Srndovic J., Roth S.V. et al. // Cellulose. 2022. V. 29. № 1. P. 117. https://doi.org/10.1007/s10570-021-04291-x
- Guild J.D., Knox S.T., Burholt S.B. et al. // Macromolecules. 2023. V. 56. № 16. P. 6426. https://doi.org/10.1021/acs.macromol.3c00585
- Porod G. // Kolloid-Zeitschrift. 1952. V. 125. № 1. P. 51. https://doi.org/10.1007/BF01519615
- Hammouda B. // J. Appl. Crystallogr. 2010. V. 43. № 4. P. 716. https://doi.org/10.1107/S0021889810015773
- Schmidt P.W., Avnir D., Levy D. et al. // J. Chem. Phys. 1991. V. 94. № 2. P. 1474. https://doi.org/10.1063/1.460006