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Vol 60, No 11-12 (2019)

Metal Science Research at the National Technology Initiative “New Production Technologies” Center of Peter the Great St. Petersburg Polytechnic University

Texture Formation in Hot Rolling of Electrical Anisotropic Steel

Rudskoy A.I., Kononov A.A., Kondrat’ev S.Y., Matveev M.A.

Abstract

Processes of structure and texture formation in hot rolling of electrical anisotropic steel are studied. It is shown that the structure of the surface layers of hot-rolled strips forms as a result of the joint action of γ → α phase transformation and dynamic recrystallization. The structure of the central layers forms as a result of recovery of deformed grains.

Metal Science and Heat Treatment. 2019;60(11-12):689-694
pages 689-694 views

Article

Effect of the Temperature of Friction Stir Welding on the Microstructure and Mechanical Properties of Welded Joints of an Al – Cu – Mg Alloy

Naumov A.A., Isupov F.Y., Golubev Y.A., Morozova Y.N.

Abstract

A method for assessing the effect of the temperature of friction stir welding on the microstructure and mechanical properties of welded joints of aluminum alloy D16AT is suggested. The temperature cycles in different zones of a welded joint are determined by mathematical simulation. The computed temperature cycles are implemented in a Gleeble-3800 system. It is shown that the welding temperature affects little the evolution of the microstructure in different zones of the welded joints of alloy D16AT.

Metal Science and Heat Treatment. 2019;60(11-12):695-700
pages 695-700 views

Tailoring the Properties in Functionally Graded Alloy Inconel 718 Using Additive Technologies

Popovich V.A., Borisov E.V., Sufiyarov V.S., Popovich A.A.

Abstract

A novel method for forming “programmed” mechanical properties in local components of a part by controlling the microstructure of the alloy under additive production is suggested. It is shown that the thermal fields acting during the additive production may be used for manipulating the preferred orientation of the growing crystals and forming different-size grains, which affects the mechanical characteristics. A gradient material from a high-temperature nickel alloy Inconel 718 with coarse elongated grains in the core and fine-grained microstructure in the external shell is produced and shown to possess higher operating characteristics than the alloy fabricated by the conventional process.

Metal Science and Heat Treatment. 2019;60(11-12):701-709
pages 701-709 views

Morphology of High-Strength Heat-Resistant Steel Powder for Machines for Additive Production from Shavings

Razumov N.G., Popovich A.A., Grigor’ev A.V., Silin A.O., Goncharov I.S.

Abstract

Results of a study of the production of spherical-shape powder from shavings of high-alloy high-temperature steel 13Kh11N2V2MF (ÉI961) are presented. It is shown that the rate of feeding of the powder into the flow of thermal plasma affects the process of spheroidization of the particles. The chemical composition of the powder is compared to that required by the GOST standard.

Metal Science and Heat Treatment. 2019;60(11-12):710-714
pages 710-714 views

A Study of Modes of Hardening Heat Treatment of Titanium Alloy VT23

Kondrat’eva O.V., Kondrat’ev S.Y., Shvetsov O.V.

Abstract

The microstructure and mechanical properties of alloy VT23 are studied after different variants of quenching and aging. The best combination of mechanical properties is obtained after 1-h water quenching from 850°C and 10-h aging at 550°C. This mode of heat treatment yields a homogeneous globular α + β structure providing high characteristics of strength, ductility and toughness.

Metal Science and Heat Treatment. 2019;60(11-12):715-721
pages 715-721 views

Effect of Medium-Temperature Additional Tempering on the Carbide Phase and Cold Resistance of Heat-Hardenable Steel 09G2SA-A

Gorynin V.I., Kondrat’ev S.Y., Olenin M.I., Mikhailov M.S.

Abstract

The interrelation between the fine structure and the cold resistance of forgings and rolled sheets from ferritic-pearlitic steel 09G2SA-A after heat hardening and additional tempering at 450°C is studied. The additional medium-temperature tempering is shown to raise effectively the cold resistance of the steel due to coagulation and spheroidization of the cementite-type carbides, which make the structure of the steel more equilibrium.

Metal Science and Heat Treatment. 2019;60(11-12):722-727
pages 722-727 views

Effect of Heat Treatment on the Structure and Phase Composition of a High-Temperature Nickel Alloy Obtained by Laser Cladding

Masaylo D.V., Orlov A.V., Igoshin S.D.

Abstract

Modes of laser cladding of heat-resistant nickel alloy Inconel 625 are considered. The gas-powder flow is studied and optimized as a function of the flow rate of the protective and transporting gas. The effect of the heat treatment modes on the structure and phase composition of the alloy is analyzed. Amode producing compact samples of the alloy is worked out.

Metal Science and Heat Treatment. 2019;60(11-12):728-733
pages 728-733 views

Microstructure and Mechanical Properties of Dissimilar Al – Cu Joints Formed by Friction Stir Welding

Ryl’kov E.N., Isupov F.Y., Naumov A.A., Panchenko O.V., Shamshurin A.I.

Abstract

Friction-stir-welded joints of commercial-purity copper and aluminum alloy AMg5 are studied. The effect of the process parameters on the microstructure and mechanical properties of the joints is analyzed. The results of temperature measurements during the welding made with the help of thermocouples are presented. A mathematical model is suggested for computing the temperature field of a weld. The computed and experimental data are compared.

Metal Science and Heat Treatment. 2019;60(11-12):734-738
pages 734-738 views

A Study of Structural Features of a Gradient Material from a Heat-Resistant Nickel Alloy Produced by Laser Cladding

Masaylo D.V., Popovich A.A., Sufiyarov V.S., Orlov A.V., Shamshurin A.I.

Abstract

Laser cladding is used to fabricate a gradient-structure sample from heat-resistant nickel alloy Inconel 625. The structure of the alloy is studied after direct growth at different laser spot diameters. The effect of the heat treatment on the gradient-structure sample is determined. EBSD images of different regions of the article are obtained and analyzed.

Metal Science and Heat Treatment. 2019;60(11-12):739-744
pages 739-744 views

Effect of Heat Treatment Modes on the Structure and Properties of Alloy VT6 After Selective Laser Melting

Sufiyarov V.S., Borisov E.V.

Abstract

The structure and mechanical properties of specimens produced by selective laser melting of a plasma-atomized powder of alloy VT6 are studied. The effect of annealing at 800 – 1050°C on the microstructure represented after the selective laser melting by a fine dispersed martensitic α′-phase and primary β-grains is considered.

Metal Science and Heat Treatment. 2019;60(11-12):745-748
pages 745-748 views

Macrostructure and Mechanical Properties of Al – Si, Al – Mg – Si, and Al – Mg – Mn Aluminum Alloys Produced by Electric Arc Additive Growth

Panchenko O.V., Zhabrev L.A., Kurushkin D.V., Popovich A.A.

Abstract

The macrostructure and mechanical properties of clad metal produced by electric arc additive growth using wires of aluminum alloys of three alloying systems (Al – Si, Al – Mg – Si, and Al – Mg – Mn) are studied. The distribution of the pores is assessed, the porosity and the microhardness are evaluated. The anisotropy of the mechanical properties determined in some specimens is explained.

Metal Science and Heat Treatment. 2019;60(11-12):749-754
pages 749-754 views

Synthesis and Investigation of Quaternary Quasi-Crystalline Phase in Al – Cu – Fe – Cr Alloys

Wang Y., Hou H., Zhao Y., Tian J.

Abstract

Formation of a quasi-crystalline phase under rapid solidification and heat treatment of alloys of the Al – Cu – Fe – Cr system is studied. The study is performed by x-ray diffractometry, optical, scanning and transmission electron microscopy and differential scanning calorimetry. It is shown that the quasi-crystalline Al65Cu20Fe10Cr5 phase is a mixture of icosahedral and decagonal phases. The substitution of iron with chromium destabilizes the icosahedral I-phase and promotes formation of a decagonal d-phase. After quenching from 880°C, the Al64Cu24Fe10Cr2 alloy acquires a pure I-phase, and the Al64Cu24Fe8Cr4 alloy acquires a d-phase.

Metal Science and Heat Treatment. 2019;60(11-12):770-776
pages 770-776 views

Determination of the Parameters of Precipitates in Aged Mg – 8% Zn – 4% Al – 0.2% Cr – 0.5% Bi Alloy

Ye J., Lin X., Dong Y., Teng F., Sun G.

Abstract

The structure of precipitates in alloy Mg – 8% Zn – 4% Al – 0.2% Cr – 0.5% Bi aged at 70 and 160°C for up to 1200 h is studied by high-resolution transmission electron microscopy. The hardness of the alloy is determined; the precipitates of the phases are identified in different aging stages.

Metal Science and Heat Treatment. 2019;60(11-12):783-787
pages 783-787 views

Nonmetallic Inclusions in Alloys of the Fe – Co – Ni – Cu – Al – Ti System with Hafnium and Niobium

Belyaev I.V., Bazhenov V.E., Moiseev A.V.

Abstract

Nonmetallic inclusions in magnetic alloys of the Fe – Co – Ni – Cu – Al – Ti system with additions of niobium and hafnium used in the production of single-crystal permanent magnets are studied. The kinds of inclusions in magnetic alloys are determined with the help of rapid analysis of the chemical composition, optical and electron microscopy, quantitative microscopic x-ray spectrum analysis, and electron back-scatter diffraction. The phase compositions are computed with the help of the Thermo-Calc software.

Metal Science and Heat Treatment. 2019;60(11-12):795-801
pages 795-801 views

Raising the Corrosion Resistance of Plasma-Nitrided Steel 45 (AISI 1045) by Preliminary Sandblasting

Miao B., Zhao X., Song L., Wei K., Hu J.

Abstract

Steel 45 (AISI 1045) is studied after a sandblasting treatment and plasma nitriding. The corrosion resistance of the steel is determined by measuring the electrochemical polarization and electrochemical impedance. The optimum time of sandblasting yielding the thickest and densest nitride layer is determined.

Metal Science and Heat Treatment. 2019;60(11-12):808-813
pages 808-813 views

A Study of Graphitization of Free-Cutting Steel

Zhang Y., Han J.

Abstract

An alternative for the traditional free-cutting steels, i.e., a graphitized steel, is suggested with allowance for the tendencies in design of free-cutting steels connected with reduction of the sulfur content and transfer to unleaded steels. The graphitization process due to inoculation of the steel with boron nitride (BN) is studied by metallography. Electron microscopy is used to determine the interaction between the boron nitride substrate and the graphite. The statistical relation between the content of the graphite phase and the duration of the graphitization process is used to show that the degree of graphitization is describable by the Avrami equation.

Metal Science and Heat Treatment. 2019;60(11-12):817-819
pages 817-819 views

Metal Science and Heat Treatment Volume 60, Number 11

Metal Science and Heat Treatment. 2019;60(11-12):687-688
pages 687-688 views

Metal Science and Heat Treatment Volume 60, Number 12

Metal Science and Heat Treatment. 2019;60(11-12):755-756
pages 755-756 views

Structure

Special Features of Structure Formation in Deposited Metal Based on Alloyed Nickel Aluminide and its High-Temperature Properties

Zorin I.V., Dubtsov Y.N., Sokolov G.N., Lysak V.I.

Abstract

Special features of structure and phase formation in deposited metal based on alloyed Ni3 Al nickel aluminide formed due to high-gradient crystallization under the conditions of the thermal cycle of arc surfacing are studied. The effect of microalloying with ultrafine WC carbides on the resistance to thermal fatigue and plastic straining at elevated temperatures (up to 1200°C) is considered.

Metal Science and Heat Treatment. 2019;60(11-12):757-763
pages 757-763 views

Aluminum Alloys

Effect of Radial Shear Rolling on the Structure and Mechanical Properties of a New-Generation High-Strength Aluminum Alloy Based on the Al – Zn – Mg – Ni – Fe System

Shurkin P.K., Akopyan T.K., Galkin S.P., Aleshchenko A.S.

Abstract

A high-strength aluminum alloy based on the Al – Zn – Mg – Ni – Fe system is studied in deformed condition after radial shear rolling with reduction 2.78 and 8.16. The microstructure and the hardness are shown to change in the process of the thermal deformation involving quenching and aging by modes T and T1. The bars deformed with reduction 8.16 have a dense gradient structure containing a surface layer with a thickness of bout 300 μm, in which the size of the fine dispersed equiaxed grains ranges within 15 – 25 μm. The high accumulated strain combined with the precipitation hardening of the alloy in state T1 is shown to provide competitive mechanical properties, i.e., an ultimate strength of 605 MPa, a yield strength of 551 MPa, and an elongation of 5.5%.

Metal Science and Heat Treatment. 2019;60(11-12):764-769
pages 764-769 views

Magnesium Alloys

Effect of Hot Rotary Swaging and Subsequent Annealing on Microstructure and Mechanical Properties of Magnesium Alloy WE43

Wang C., Yu Z., Cui Y., Yu S., Ma X., Liu H.

Abstract

The effect of hot rotary swaging and subsequent annealing on the microstructure and mechanical properties of magnesium alloy WE43 of the Mg – Y – Nd – Zr system is studied. The optimum temperature of rotary swaging providing refinement of the microstructure, change in the preferential grain orientation, strain hardening and growth in the strength is determined. It is shown that subsequent annealing at 400°C for 60 min raises the ductility, causes the appearance of equiaxed grains, and removes the strain hardening, which makes it possible to perform further deformation.

Metal Science and Heat Treatment. 2019;60(11-12):777-782
pages 777-782 views

Refractory and Magnetic Alloys

Crystallographic Structure of Alloy ZhS32-VI Obtained by Selective Laser Melting of Powder Composition on Single-Crystal Substrate

Treninknov I.A., Petrushin N.V., Evgenov A.G.

Abstract

The crystallographic structure, the phase composition, and the microstructure of refractory nickel alloy ZhS32-VI fabricated by selective laser melting of a powder composition on single-crystal stub substrates with crystallographic orientations 〈001〉 and 〈111〉 are studied.

Metal Science and Heat Treatment. 2019;60(11-12):788-794
pages 788-794 views

Treatment

Investigation of the Structure and Properties of Steel 30KhGSA after Volume Laser-Beam Treatment

Kuryntsev S.V., Morushkin A.E., Shigapov A.I.

Abstract

Results of a study of billets from steel 30KhGSA after a volume laser treatment, which consists of high-speed (20 mm/sec) remelting of a metallic plate with a thickness of 10 mm by a laser beam, are presented. It has been expected that this treatment process should yield a laser-beam-remelted gradient layer with changed microstructure due to the high cooling rate.

Metal Science and Heat Treatment. 2019;60(11-12):802-807
pages 802-807 views

Technical Information

Crack Resistance of Volume-Hardened Railroad Rails with Transverse Cracks in the Head

Georgiev M.N., Simeonova T.V.

Abstract

The crack resistance of railroad rails with transverse internal and external cracks in the head formed in operation is determined. The ultimate crack resistance Ic, the values of which coincide with the critical values of the stress intensity factor KIc under the brittle fracture typical for rails, is determined.

Metal Science and Heat Treatment. 2019;60(11-12):814-816
pages 814-816 views

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