Email this article Synthesis of preceramic organomagnesiumoxanealumoxanes
- Authors: Shcherbakova G.I.1, Storozhenko P.A.1, Krivtsova N.S.1, Kutinova N.B.1, Apukhtina T.L.1, Varfolomeev M.S.1, Kuznetsova M.G.1, Drachev A.I.1, Stolyarova I.V.1, Ashmarin A.A.2
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Affiliations:
- State Research Institute for Chemistry and Technology of Organoelement Compounds
- Baikov Institute of Metallurgy and Materials Science
- Issue: Vol 53, No 11 (2017)
- Pages: 1209-1216
- Section: Article
- URL: https://journals.rcsi.science/0020-1685/article/view/158329
- DOI: https://doi.org/10.1134/S0020168517110103
- ID: 158329
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Abstract
Preceramic organomagnesiumoxanealumoxanes hydrolytically stable in air and soluble in organic solvents, exhibiting fiber-forming properties at Al: Mg molar ratios of 2: 1 and 1: 1, have been synthesized for the first time. The physicochemical properties of the organomagnesiumoxanealumoxanes and ceramic samples prepared from them have been studied by a variety of techniques (nuclear magnetic resonance, IR spectroscopy, scanning electron microscopy, thermogravimetric analysis, X-ray diffraction, and elemental analysis).
About the authors
G. I. Shcherbakova
State Research Institute for Chemistry and Technology of Organoelement Compounds
Author for correspondence.
Email: eos2004@inbox.ru
Russian Federation, sh. Entuziastov 38, Moscow, 105118
P. A. Storozhenko
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: eos2004@inbox.ru
Russian Federation, sh. Entuziastov 38, Moscow, 105118
N. S. Krivtsova
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: eos2004@inbox.ru
Russian Federation, sh. Entuziastov 38, Moscow, 105118
N. B. Kutinova
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: eos2004@inbox.ru
Russian Federation, sh. Entuziastov 38, Moscow, 105118
T. L. Apukhtina
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: eos2004@inbox.ru
Russian Federation, sh. Entuziastov 38, Moscow, 105118
M. S. Varfolomeev
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: eos2004@inbox.ru
Russian Federation, sh. Entuziastov 38, Moscow, 105118
M. G. Kuznetsova
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: eos2004@inbox.ru
Russian Federation, sh. Entuziastov 38, Moscow, 105118
A. I. Drachev
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: eos2004@inbox.ru
Russian Federation, sh. Entuziastov 38, Moscow, 105118
I. V. Stolyarova
State Research Institute for Chemistry and Technology of Organoelement Compounds
Email: eos2004@inbox.ru
Russian Federation, sh. Entuziastov 38, Moscow, 105118
A. A. Ashmarin
Baikov Institute of Metallurgy and Materials Science
Email: eos2004@inbox.ru
Russian Federation, Leninskii pr. 49, Moscow, 119991
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