Determination of Particle Size Distribution of Zirconium Dioxide Powders by Static Laser Scattering and Optical Microscopy

Abstract

Dispersing conditions of powdered zirconium dioxide with addition of 3 mol % yttrium oxide are determined. The particle size distribution of the powders is determined by static laser scattering and optical microscopy. The zeta potential of suspension of zirconium dioxide particles as a function of pH of medium is measured by electrophoresis with titration. The influence of acidity on suspension stability during measurements is studied. It is demonstrated that a stable suspension can be obtained by shift of pH to both the acid and alkaline regions as well as by addition of surfactants, such as Dolapix CE 64.