Email this article Th e Relationship between the Particle Size Distribution of Aluminum Powder and the Structural-Phase Composition and Properties of the Al2O3—AlN Coating Formed under the Infl uence of Electric Arc Nitrogen Plasma
- Authors: Volchkov I.S.1, Podkur P.L.1, Muslimov A.E.1, Gadzhiev M.K.2, Ilyichev M.V.2, Kanevsky V.M.1
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Affiliations:
- Kurchatov Complex of Crystallography and Photonics
- Joint Institute for High Temperatures, RAS
- Issue: Vol 123, No 3-4 (2024): THEMED SECTION: STRUCTURAL DIAGNOSTICS OF MATERIALS
- Pages: 60-67
- Section: THEMED SECTION: FUNDAMENTAL SCIENTIFIC RESEARCH IN THE FIELD OF NATURAL SCIENCES
- URL: https://journals.rcsi.science/1605-8070/article/view/303513
- DOI: https://doi.org/10.22204/2410-4639-2024-123-124-03-04-60-67
- ID: 303513
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Abstract
The relationship between the particle size distribution of aluminum powder and the structural-phase composition and properties of the Al2O3–AlN coating formed under the influence of electric arc plasma has been studied. Two types of Al powders were used: micropowder with a particle size of ~20–120 μm and nanopowder with a particle size of ~40–100 nm. It was found that coatings obtained from Al micropowder are agglomerates of pure Al interspersed with AlN and Al5O6N clusters. Coatings obtained from Al nanopowder contain Al2O3 as a base interspersed with AlN and Al5O6N agglomerates, as well as a noticeable proportion of unreacted Al. The surface morphology of the samples is heterogeneous and porous. In the process of measuring microhardness using the indentation method, a correlation with the local phase composition of the surface was discovered. The Al2O3 and AlN phases had the highest microhardness, about 9.097±0.324 GPa and 17.800±0.674 GPa, respectively. The results obtained demonstrate the promise of applying Al2O3–AlN coatings using low-temperature plasma to improve the service life of steel structures.
About the authors
Ivan S. Volchkov
Kurchatov Complex of Crystallography and Photonics
Author for correspondence.
Email: Volch2862@gmail.com
Russian Federation, 59 Leninsky Ave., Moscow, 119333, Russia
Pavel L. Podkur
Kurchatov Complex of Crystallography and Photonics
Email: vverde85@yandex.ru
Russian Federation, 59 Leninsky Ave., Moscow, 119333, Russia
Arsen E. Muslimov
Kurchatov Complex of Crystallography and Photonics
Email: amuslimov@mail.ru
Russian Federation, 59 Leninsky Ave., Moscow, 119333, Russia
Makhach Kh. Gadzhiev
Joint Institute for High Temperatures, RAS
Email: makhach@mail.ru
Russian Federation, 13 Bd. 2, Izhorskaya Str., Moscow, 125412, Russia
Maxim V. Ilyichev
Joint Institute for High Temperatures, RAS
Email: imvpl@mail.ru
Russian Federation, 13 Bd. 2, Izhorskaya Str., Moscow, 125412, Russia
Vladimir M. Kanevsky
Kurchatov Complex of Crystallography and Photonics
Email: kanev@crys.ras.ru
Russian Federation, 59 Leninsky Ave., Moscow, 119333, Russia
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