Email this article Synthesis and characterization of nanocomposites Fe3O4–SiO2–chitosan based on lbl technology
- Authors: Yang Y.1,2, Liu X.3, Xu H.1, Shi H.2
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Affiliations:
- School of Chemical and Environmental Engineering
- School of Chemistry and Molecular Engineering
- Analysis Test Center
- Issue: Vol 42, No 3 (2016)
- Pages: 312-321
- Section: Article
- URL: https://journals.rcsi.science/1087-6596/article/view/215571
- DOI: https://doi.org/10.1134/S1087659616030056
- ID: 215571
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Abstract
In this paper, the apparent chain-like core-shell structure Fe3O4–SiO2–chitosan nanoparticles was synthesized by two-step method with cross-linking action of glutaraldehyde based on layer-by-layer technology, the composite particles were characterized by IR, XRD, TEM, SEM, EDS and VSM analytical methods, and the synthesis conditions of the product were studied. The results indicated that the diameter of the composite particles is about 106.5 nm, the parietal layer of chitosan is 20 nm, and after crosslinking action of glutaraldehyde, chitosan uniformaly coated the outer surface of Fe3O4–SiO2.
About the authors
Yuxiang Yang
School of Chemical and Environmental Engineering; School of Chemistry and Molecular Engineering
Author for correspondence.
Email: yxyang@ecust.edu.cn
China, Shanghai, 201418; Shanghai, 200237
Xiangnong Liu
Analysis Test Center
Email: yxyang@ecust.edu.cn
China, Yangzhou, 225009
Hailan Xu
School of Chemical and Environmental Engineering
Email: yxyang@ecust.edu.cn
China, Shanghai, 201418
Haowei Shi
School of Chemistry and Molecular Engineering
Email: yxyang@ecust.edu.cn
China, Shanghai, 200237
