Improving the Chemical Purity of Fused Corundum by High-Temperature Roasting
- Authors: Belyaev G.E.1, Vlaskin M.S.1, Grigorenko A.V.1, Zhuk A.Z.1, Lipatova I.A.1, Shkol’nikov E.I.1
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Affiliations:
- Joint Institute for High Temperatures, Russian Academy of Sciences
- Issue: Vol 59, No 6 (2019)
- Pages: 648-653
- Section: Article
- URL: https://journals.rcsi.science/1083-4877/article/view/249189
- DOI: https://doi.org/10.1007/s11148-019-00289-y
- ID: 249189
Cite item
Abstract
The chemical purity of fused corundum was demonstrated experimentally to improve after high-temperature (~1750°C) vacuum (~10–5 mm Hg) roasting. Three industrial fused corundum samples with different particle-size and impurity profiles were heat treated, after which the impurity contents decreased by an order of magnitude. The samples were practically completely purified of Na, Mg, K, Mn, Cu, and Zn whereas the Fe content decreased by 8 – 10 times. Samples were found to consist of porous granules 16 – 60 μm in size that consisted of solid microparticles of characteristic size 0.4 – 0.7 μm. The specific surface area of the granules lay in the range 2.8 – 3.3 cm2/g.
About the authors
G. E. Belyaev
Joint Institute for High Temperatures, Russian Academy of Sciences
Email: 666zhuk@ihed.ras.ru
Russian Federation, Moscow
M. S. Vlaskin
Joint Institute for High Temperatures, Russian Academy of Sciences
Email: 666zhuk@ihed.ras.ru
Russian Federation, Moscow
A. V. Grigorenko
Joint Institute for High Temperatures, Russian Academy of Sciences
Email: 666zhuk@ihed.ras.ru
Russian Federation, Moscow
A. Z. Zhuk
Joint Institute for High Temperatures, Russian Academy of Sciences
Author for correspondence.
Email: 666zhuk@ihed.ras.ru
Russian Federation, Moscow
I. A. Lipatova
Joint Institute for High Temperatures, Russian Academy of Sciences
Email: 666zhuk@ihed.ras.ru
Russian Federation, Moscow
E. I. Shkol’nikov
Joint Institute for High Temperatures, Russian Academy of Sciences
Email: 666zhuk@ihed.ras.ru
Russian Federation, Moscow