Synthesis of  N -Aryl- and  N,N -diethyl-2-methyl-3-phenyl-4-sulfanylidene-3,4,5,6-tetrahydro-2 H -2,6-methano-1,3,5-benzoxadiazocine-11-carboxamides

V. L. Gein; T. M. Zamaraeva; N. A. Buzmakova; M. V. Dmitriev; O. E. Nasakin; M. I. Kazantseva

doi:10.1134/S1070428017010158

Synthesis of N-Aryl- and N,N-diethyl-2-methyl-3-phenyl-4-sulfanylidene-3,4,5,6-tetrahydro-2H-2,6-methano-1,3,5-benzoxadiazocine-11-carboxamides

Autores: Gein V.L.¹, Zamaraeva T.M.¹, Buzmakova N.A.¹, Dmitriev M.V.², Nasakin O.E.³, Kazantseva M.I.³
Afiliações:
1. Perm State Pharmaceutical Academy
2. Perm National State Research University
3. I.N. Ul’yanov Chuvash State University
Edição: Volume 53, Nº 1 (2017)
Páginas: 86-89
Seção: Article
URL: https://journals.rcsi.science/1070-4280/article/view/215647
DOI: https://doi.org/10.1134/S1070428017010158
ID: 215647

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Resumo

N-Aryl- and N,N-diethyl-3-oxobutanamides reacted with salicylaldehyde and N-phenylthiourea in ethanol in the presence of sodium hydrogen sulfate as catalyst to give the corresponding N-substituted 2-methyl-3-phenyl-4-sulfanylidene-3,4,5,6-tetrahydro-2H-2,6-methano-1,3,5-benzoxadiazocine-11-carboxamides.