Отправить статью по E-mail Synthesis of 1-[4-(1,3-diaryl-4,5-dihydro-1H-pyrazol-5-yl)-2,3,5,6-tetrafluorophenyl]piperidin-4-ols and their acrylates
- Авторы: Soboleva E.A.1, Orlova N.A.1, Shelkovnikov V.V.1,2
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Учреждения:
- Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch
- Novosibirsk State Technical University
- Выпуск: Том 53, № 3 (2017)
- Страницы: 398-406
- Раздел: Article
- URL: https://journals.rcsi.science/1070-4280/article/view/215925
- DOI: https://doi.org/10.1134/S1070428017030149
- ID: 215925
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Аннотация
(4-Hydroxypiperidin-1-yl)tetra- and -octafluorochalcones reacted with phenylhydrazine in acetic acid to give mixtures of polyfluoro-1,3,5-triaryl-4,5-dihydro-1H-pyrazoles and their O-acetyl derivatives. Analogous reactions in ethanol afforded in satisfactory yields 1-[4-(1,3-diaryl-4,5-dihydro-1H-pyrazol-5-yl)-2,3,5,6-tetrafluorophenyl]piperidin-4-ols which were treated with acryloyl chloride to obtain the corresponding acrylates that are promising as monomers for the preparation of fluorescent films.
Об авторах
E. Soboleva
Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch
Email: ona@nioch.nsc.ru
Россия, pr. Akademika Lavrent’eva 9, Novosibirsk, 630090
N. Orlova
Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch
Автор, ответственный за переписку.
Email: ona@nioch.nsc.ru
Россия, pr. Akademika Lavrent’eva 9, Novosibirsk, 630090
V. Shelkovnikov
Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch; Novosibirsk State Technical University
Email: ona@nioch.nsc.ru
Россия, pr. Akademika Lavrent’eva 9, Novosibirsk, 630090; pr. Karla Marksa 20, Novosibirsk, 630073
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