Synthesis of (3-Hydroxyadamantan-1-yl)methanols


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A convenient procedure has been developed for the synthesis of (3-hydroxyadamantan-1-yl)-methanols on the basis of nitroxylation of adamantan-1-ylmethanols with fuming nitring acid and subsequent reduction of intermediate nitric acid esters with hydrazine hydrate. The title diols have also been obtained by the reduction of 1-nitroxy-3-(nitroxymethyl)adamantanes. The nitroxylation process is accompanied by oxidation with the formation of substituted adamantane-1-carboxylic acids.

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E. Ivleva

Samara State Technical University

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Email: elena.a.ivleva@yandex.com
俄罗斯联邦, ul. Molodogvardeiskaya 244, Samara, 443100

A. Pogulyaiko

Samara State Technical University

Email: elena.a.ivleva@yandex.com
俄罗斯联邦, ul. Molodogvardeiskaya 244, Samara, 443100

Yu. Klimochkin

Samara State Technical University

Email: elena.a.ivleva@yandex.com
俄罗斯联邦, ul. Molodogvardeiskaya 244, Samara, 443100

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