Efficient synthesis of cyclophanes containing sulfur and nitrogen atoms by cycloaminomethylation of benzenedithiols in the presence of samarium-based catalysts

N. N. Makhmudiyarova; G. M. Kiyamutdinova; E. S. Meshcheryakova; A. G. Ibragimov; U. M. Dzhemilev

doi:10.1134/S1070428016100080

Efficient synthesis of cyclophanes containing sulfur and nitrogen atoms by cycloaminomethylation of benzenedithiols in the presence of samarium-based catalysts

Authors: Makhmudiyarova N.N.¹, Kiyamutdinova G.M.¹, Meshcheryakova E.S.¹, Ibragimov A.G.¹, Dzhemilev U.M.¹
Affiliations:
1. Institute of Petrochemistry and Catalysis
Issue: Vol 52, No 10 (2016)
Pages: 1419-1426
Section: Article
URL: https://journals.rcsi.science/1070-4280/article/view/215028
DOI: https://doi.org/10.1134/S1070428016100080
ID: 215028

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Abstract

An efficient procedure has been developed for the synthesis of 3-aryl-3,4-dihydro-2H-1,5,3-benzodithiazepines, 4-aryl-2,6-dithia-4-azabicyclo[5.3.1]undeca-1(11),7,9-trienes, and 4,10,16-triaryl-2,6,8,12,14,18-hexathia-4,10,16-triaza-1,7,13(1,4)-tribenzenacyclooctadecaphanes by samarium-catalyzed cycloaminomethylation of benzenedithiols with N,N-bis(methoxymethyl)anilines.