Reaction of thiourea with formaldehyde and simplest aliphatic diamines
- 作者: Hamoud F.1, Ramsh S.M.1, Fundamenskii V.S.1, Gurzhii V.V.2, Brusina M.A.1, Arkhipova N.G.1,2, Sedunova P.A.1, Medvedskii N.L.1, Khrabrova E.S.1
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隶属关系:
- St. Petersburg State Institute of Technology
- St. Petersburg State University
- 期: 卷 52, 编号 1 (2016)
- 页面: 121-126
- 栏目: Article
- URL: https://journals.rcsi.science/1070-4280/article/view/213609
- DOI: https://doi.org/10.1134/S1070428016010231
- ID: 213609
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详细
N,N′-Bis(hydroxymethyl)thiourea reacted with propane-1,3-diamine at a molar ratio of 2 : 1 to give 5,5′-propane-1,3-diylbis(1,3,5-triazinane-2-thione), whereas 1,3,5,7,11,13,15,17-octaazatricyclo[15.3.1.17,11]-docosane-4,14-dithione was obtained in the reaction with equimolar amounts of the reactants. Tricyclic product was also formed in the three-component condensation of thiourea with formaldehyde and propane-1,3-diamine at a ratio of 1 : 3 : 1. The reactions of N,N′-bis(hydroxymethyl)thiourea with ethane-1,2-diamine (2 : 1) and of thiourea with formaldehyde and butane-1,4-diamine (1 : 2 : 1) afforded 5,5′-(ethane-1,2-diyl)bis(1,3,5-triazinane-2-thione) and 5,5′-(butane-1,4-diyl)bis(1,3,5-triazinane-2-thione), respectively.
作者简介
F. Hamoud
St. Petersburg State Institute of Technology
编辑信件的主要联系方式.
Email: fares_hamoud26@yahoo.fr
俄罗斯联邦, Moskovskii pr. 26, St. Petersburg, 190013
S. Ramsh
St. Petersburg State Institute of Technology
Email: fares_hamoud26@yahoo.fr
俄罗斯联邦, Moskovskii pr. 26, St. Petersburg, 190013
V. Fundamenskii
St. Petersburg State Institute of Technology
Email: fares_hamoud26@yahoo.fr
俄罗斯联邦, Moskovskii pr. 26, St. Petersburg, 190013
V. Gurzhii
St. Petersburg State University
Email: fares_hamoud26@yahoo.fr
俄罗斯联邦, Universitetskii pr. 26, St. Petersburg, 198504
M. Brusina
St. Petersburg State Institute of Technology
Email: fares_hamoud26@yahoo.fr
俄罗斯联邦, Moskovskii pr. 26, St. Petersburg, 190013
N. Arkhipova
St. Petersburg State Institute of Technology; St. Petersburg State University
Email: fares_hamoud26@yahoo.fr
俄罗斯联邦, Moskovskii pr. 26, St. Petersburg, 190013; Universitetskii pr. 26, St. Petersburg, 198504
P. Sedunova
St. Petersburg State Institute of Technology
Email: fares_hamoud26@yahoo.fr
俄罗斯联邦, Moskovskii pr. 26, St. Petersburg, 190013
N. Medvedskii
St. Petersburg State Institute of Technology
Email: fares_hamoud26@yahoo.fr
俄罗斯联邦, Moskovskii pr. 26, St. Petersburg, 190013
E. Khrabrova
St. Petersburg State Institute of Technology
Email: fares_hamoud26@yahoo.fr
俄罗斯联邦, Moskovskii pr. 26, St. Petersburg, 190013
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