Synthesis of tertiary amines containing gem-dichlorocyclopropane and cycloacetal fragments
- Авторы: Raskil’dina G.Z.1, Valiev V.F.1, Zlotskii S.S.1
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Учреждения:
- Ufa State Petroleum Technological University
- Выпуск: Том 89, № 5 (2016)
- Страницы: 753-757
- Раздел: Organic Synthesis and Industrial Organic Chemistry
- URL: https://journals.rcsi.science/1070-4272/article/view/213858
- DOI: https://doi.org/10.1134/S1070427216050116
- ID: 213858
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Аннотация
Reactions of secondary amines containing gem-dichlorocyclopropane and cycloacetal fragments with allyl chloride, trans-1,3-dichloropropene, benzyl chloride, and chloromethyl-gem-dichlorocyclopropane were studied. The corresponding tertiary amines were obtained in 20–85% yield. Microwave radiation stimulates N-alkylation of the secondary amine containing the heterocyclic moiety. The structures of the tertiary amines prepared were studied. The configuration of the double bond in the trans-1,3-dichloropropene derivative is retained.
Об авторах
G. Raskil’dina
Ufa State Petroleum Technological University
Автор, ответственный за переписку.
Email: graskildina444@mail.ru
Россия, ul. Kosmonavtov 1, Ufa, Bashkortostan, 450062
V. Valiev
Ufa State Petroleum Technological University
Email: graskildina444@mail.ru
Россия, ul. Kosmonavtov 1, Ufa, Bashkortostan, 450062
S. Zlotskii
Ufa State Petroleum Technological University
Email: graskildina444@mail.ru
Россия, ul. Kosmonavtov 1, Ufa, Bashkortostan, 450062
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