Preparation of Dodecyl Dimethyl Benzyl Ammonium Bromide-Doped Cubic CaCO3 with Antibacterial Properties


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CaCl2 encapsulated was placed in the hydrothermal reactor of an aqueous solution of Na2CO3 and dodecyl dimethyl benzyl ammonium bromide for synthesis of two samples of calcium carbonate by an improved hydrothermal method and one-pot method. Their crystal structure, morphology, chemical composition, and thermal stability of the synthesized samples of calcium carbonate were investigated by XRD, FTIR, SEM, EDS and TGDSC. The sterilization activity of the as-prepared samples was evaluated by killing of Sarcina lutea bacteria. The results indicated that the regular cube capsule-assisted calcium carbonate prepared by hydrothermal process was doped with dodecyl dimethyl benzyl ammonium bromide. Under the same condition, the spindle-shaped calcium carbonate synthesized the one-pot method was not doped with dodecyl dimethyl benzyl ammonium bromide. Among the samples of calcium carbonate, capsule-assisted calcium carbonate had shown better antibacterial effect for Sarcina lutea: in 48 h after its inhibition a zone diameter was 12.3 mm.

作者简介

Yong Xie

School of Chemistry & Chemical Engineering; Key Lab of Spin Electron and Nano Materials of Anhui Higher Education Institutes; Fine Chemical Product Development Research Institute

编辑信件的主要联系方式.
Email: szxieyong@126.com
中国, Suzhou, 234000; Suzhou, 234000; Suzhou, 234000

Cun Ma

School of Chemistry & Chemical Engineering

Email: szxieyong@126.com
中国, Suzhou, 234000

Zi Yang

School of Chemistry & Chemical Engineering

Email: szxieyong@126.com
中国, Suzhou, 234000

Xiang Liu

School of Chemistry & Chemical Engineering

Email: szxieyong@126.com
中国, Suzhou, 234000

Yang Wang

School of Chemistry & Chemical Engineering

Email: szxieyong@126.com
中国, Suzhou, 234000

Dian Li

School of Chemistry & Chemical Engineering

Email: szxieyong@126.com
中国, Suzhou, 234000

Hongyan Wang

Fine Chemical Product Development Research Institute

Email: szxieyong@126.com
中国, Suzhou, 234000

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