Synthesis and Characterization of Novel Magnetic Poly(urethane-imide)/Fe3O4@SiO2–NH2 Nanocomposites
- Authors: Pooladian B.1, Nikje M.M.1
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Affiliations:
- Department of Chemistry, Faculty of Science
- Issue: Vol 91, No 4 (2018)
- Pages: 671-679
- Section: Various Technological Processes
- URL: https://journals.rcsi.science/1070-4272/article/view/215802
- DOI: https://doi.org/10.1134/S1070427218040213
- ID: 215802
Cite item
Abstract
Poly(urethane-imide)/Fe3O4@SiO2–NH2 nanocomposites were synthesized by the reaction of 4,4′-diphenylmethane diisocyanate (MDI), polypropylene glycol (PPG), 4,4'-(hexafluoroisopropylidene) diphthalic anhydride and Fe3O4@SiO2–NH2 nanoparticles in propylene carbonate (PC) as an alternative green solvent. Poly(urethane-imide)s combined with Fe3O4@SiO2–NH2 nanoparticles (NPs) at various NPs ranging from loadings levels of 0.5 and 3.5 pbw were prepared and characterized by fourier transform infrared spectroscopy (FT-IR), proton nuclear magnetic resonance spectroscopy (1H NMR), thermogravimetric analysis (TGA), X-ray diffraction (XRD) and vibrating sample magnetometery (VSM). The results showed the performances of Fe3O4@SiO2–NH2 nanoparticles in improving of thermal resistance and magnetic properties of PUI/Fe3O4@SiO2–NH2 in comparison with pristine poly(urethane-imide).
About the authors
Baharak Pooladian
Department of Chemistry, Faculty of Science
Email: drmm.alavi@gmail.com
Iran, Islamic Republic of, Qazvin
Mir Mohammad Alavi Nikje
Department of Chemistry, Faculty of Science
Author for correspondence.
Email: drmm.alavi@gmail.com
Iran, Islamic Republic of, Qazvin
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