Email this article Effect of Thermal Treatment on the Structure and Properties of Hydroxyapatite
- Authors: Dobrovol’skaya I.P.1,2, Tsarev N.S.1, Osmolovskaya O.M.3, Kasatkin I.A.3, Ivan’kova E.M.1,2, Popova E.N.2, Pankova G.A.2, Yudin V.E.1,2
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Affiliations:
- Peter-the-Great St. Petersburg Polytechnical University
- Institute of Macromolecular Compounds
- St. Petersburg State University
- Issue: Vol 91, No 3 (2018)
- Pages: 368-374
- Section: Inorganic Synthesis and Industrial Inorganic Chemistry
- URL: https://journals.rcsi.science/1070-4272/article/view/215702
- DOI: https://doi.org/10.1134/S1070427218030035
- ID: 215702
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Abstract
X-ray diffraction analysis and transmission electron microscopy were used to demonstrate that hydroxyapatite produced by the precipitation method is a powder composed of anisometric particles with longitudinal size of 70–100 nm and transverse size of 7–9 nm. The particles are constituted by crystallites with longitudinal sizes of 22–24 nm and transverse sizes of 8–10 nm. At a temperature of 600°C, the crystallite sizes grow, and the volume porosity and specific surface area decrease. Synthetic hydroxyapatite has a low thermal stability as compared with hydroxyapatite of biological origin.
About the authors
I. P. Dobrovol’skaya
Peter-the-Great St. Petersburg Polytechnical University; Institute of Macromolecular Compounds
Author for correspondence.
Email: zair2@mail.ru
Russian Federation, Politekhnicheskaya 29, St. Petersburg, 195251; Bolshoy pr. 31, St. Petersburg, 199004
N. S. Tsarev
Peter-the-Great St. Petersburg Polytechnical University
Email: zair2@mail.ru
Russian Federation, Politekhnicheskaya 29, St. Petersburg, 195251
O. M. Osmolovskaya
St. Petersburg State University
Email: zair2@mail.ru
Russian Federation, St. Petersburg
I. A. Kasatkin
St. Petersburg State University
Email: zair2@mail.ru
Russian Federation, St. Petersburg
E. M. Ivan’kova
Peter-the-Great St. Petersburg Polytechnical University; Institute of Macromolecular Compounds
Email: zair2@mail.ru
Russian Federation, Politekhnicheskaya 29, St. Petersburg, 195251; Bolshoy pr. 31, St. Petersburg, 199004
E. N. Popova
Institute of Macromolecular Compounds
Email: zair2@mail.ru
Russian Federation, Bolshoy pr. 31, St. Petersburg, 199004
G. A. Pankova
Institute of Macromolecular Compounds
Email: zair2@mail.ru
Russian Federation, Bolshoy pr. 31, St. Petersburg, 199004
V. E. Yudin
Peter-the-Great St. Petersburg Polytechnical University; Institute of Macromolecular Compounds
Email: zair2@mail.ru
Russian Federation, Politekhnicheskaya 29, St. Petersburg, 195251; Bolshoy pr. 31, St. Petersburg, 199004
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