1H NMR spectra and crystal structure of the nickel(II) complex with ethyl 5,5-dimethyl-2,4-dioxohexanoate aroylhydrazones


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Abstract

Nickel(II) complexes NiLn ∙ NH3 (n = 1–5) with the products of condensation of ethyl 5,5-dimethyl-2,4-dioxohexanoate with aromatic acid hydrazides (H2L1–H2L5) were synthesized. The complexes were studied by elemental analysis and IR and 1H NMR spectroscopy. The structure of the complex NiL1 ∙ NH3 was determined by X-ray diffraction (CIF file CCDC no. 1057268).

About the authors

M. A. Tursunov

Bukhara State University

Author for correspondence.
Email: tursunovma@mail.ru
Uzbekistan, Bukhara

K. G. Avezov

Bukhara State University

Email: tursunovma@mail.ru
Uzbekistan, Bukhara

B. B. Umarov

Bukhara State University

Email: tursunovma@mail.ru
Uzbekistan, Bukhara

N. A. Parpiev

Bukhara State University

Email: tursunovma@mail.ru
Uzbekistan, Bukhara

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