1H NMR spectra and crystal structure of the nickel(II) complex with ethyl 5,5-dimethyl-2,4-dioxohexanoate aroylhydrazones
- Authors: Tursunov M.A.1, Avezov K.G.1, Umarov B.B.1, Parpiev N.A.1
-
Affiliations:
- Bukhara State University
- Issue: Vol 43, No 2 (2017)
- Pages: 93-96
- Section: Article
- URL: https://journals.rcsi.science/1070-3284/article/view/213760
- DOI: https://doi.org/10.1134/S1070328417020087
- ID: 213760
Cite item
Abstract
Nickel(II) complexes NiLn ∙ NH3 (n = 1–5) with the products of condensation of ethyl 5,5-dimethyl-2,4-dioxohexanoate with aromatic acid hydrazides (H2L1–H2L5) were synthesized. The complexes were studied by elemental analysis and IR and 1H NMR spectroscopy. The structure of the complex NiL1 ∙ NH3 was determined by X-ray diffraction (CIF file CCDC no. 1057268).
Keywords
About the authors
M. A. Tursunov
Bukhara State University
Author for correspondence.
Email: tursunovma@mail.ru
Uzbekistan, Bukhara
K. G. Avezov
Bukhara State University
Email: tursunovma@mail.ru
Uzbekistan, Bukhara
B. B. Umarov
Bukhara State University
Email: tursunovma@mail.ru
Uzbekistan, Bukhara
N. A. Parpiev
Bukhara State University
Email: tursunovma@mail.ru
Uzbekistan, Bukhara
Supplementary files
