Molecular and Crystal Structure of the Cocrystal of p-n-Heptyloxybenzoic Acid‒p-n-Hexyloxybenzoic Acid, Obtained in the System of Mesomorphic Acids
- 作者: Nosikova L.1,2, Kochetov A.1, Kudryashova Z.1,2, Melnikov A.3, Churakov A.4, Kuzmina L.4
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隶属关系:
- MIREA – Russian Technological University (M.V. Lomonosov Institute of Fine Chemical Technologies)
- Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences
- St. Petersburg State University
- Institute of General and Inorganic Chemistry, Russian Academy of Sciences
- 期: 卷 63, 编号 6 (2018)
- 页面: 909-915
- 栏目: Structure of Organic Compounds
- URL: https://journals.rcsi.science/1063-7745/article/view/193116
- DOI: https://doi.org/10.1134/S1063774518060238
- ID: 193116
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详细
The structure of the p-n-heptyloxybenzoic acid–p-n-hexyloxybenzoic acid crystal, obtained in the dual system of homologues of p-n-alkyloxybenzoic acids exhibiting mesomorphic properties has been studied by X-ray diffraction analysis at a temperature of 120 K. The crystals are triclinic, sp. gr. P\(\bar {1}\), a = 4.6380(7) Å, b = 8.0158(12) Å, c= 17.673(3) Å, α = 81.019(7)°, β = 85.632(7)°, γ = 76.935(7)°, Z = 2. The molecules in the cocrystal are combined in dimers by hydrogen bonds. The probability and conditions of the formation of cocrystals of the 1 : 1 and 1 : 2 compositions in such systems are discussed.
作者简介
L. Nosikova
MIREA – Russian Technological University (M.V. Lomonosov Institute of Fine Chemical Technologies); Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences
Email: kuzmina@igic.ras.ru
俄罗斯联邦, Moscow, 119571; Moscow, 119071
A. Kochetov
MIREA – Russian Technological University (M.V. Lomonosov Institute of Fine Chemical Technologies)
Email: kuzmina@igic.ras.ru
俄罗斯联邦, Moscow, 119571
Z. Kudryashova
MIREA – Russian Technological University (M.V. Lomonosov Institute of Fine Chemical Technologies); Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences
Email: kuzmina@igic.ras.ru
俄罗斯联邦, Moscow, 119571; Moscow, 119071
A. Melnikov
St. Petersburg State University
Email: kuzmina@igic.ras.ru
俄罗斯联邦, St. Petersburg, 199034
A. Churakov
Institute of General and Inorganic Chemistry, Russian Academy of Sciences
Email: kuzmina@igic.ras.ru
俄罗斯联邦, Moscow, 119991
L. Kuzmina
Institute of General and Inorganic Chemistry, Russian Academy of Sciences
编辑信件的主要联系方式.
Email: kuzmina@igic.ras.ru
俄罗斯联邦, Moscow, 119991