Evaluation of the Solution Stability When Reconstructing the Volume Particle Size Distribution from Small-Angle X-Ray Scattering Data for a Silicasol Solution


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Abstract

The results of studying the stability of the solution to the problem for determining the volume nanoparticle size distribution using experimental small-angle X-ray scattering (SAXS) data for a silicasol solution are presented. The possibility of reconstructing solutions using indirect Fourier transform and nonlinear minimization methods for a two-component model of spherical polydisperse particles has been investigated. The results obtained are compared with the simulation data obtained previously for theoretical data sets.

About the authors

A. E. Kryukova

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”; National Research Centre “Kurchatov Institute,”

Author for correspondence.
Email: KrukovaAE@yandex.ru
Russian Federation, Moscow, 119333; Moscow, 123182

A. S. Kozlova

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”

Email: KrukovaAE@yandex.ru
Russian Federation, Moscow, 119333

P. V. Konarev

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”; National Research Centre “Kurchatov Institute,”

Email: KrukovaAE@yandex.ru
Russian Federation, Moscow, 119333; Moscow, 123182

V. V. Volkov

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”

Email: KrukovaAE@yandex.ru
Russian Federation, Moscow, 119333

V. E. Asadchikov

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”

Email: KrukovaAE@yandex.ru
Russian Federation, Moscow, 119333

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