Email this article Iodine-Assisted Solid-State Synthesis and Characterization of Nanocrystalline Zirconium Diboride Nanosheets
- Authors: Wang L.1, Zhao D.1, Cheng Q.1, Lu Q.1, Liu W.1, Bao K.2, Zhu B.1, Zhou Q.1
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Affiliations:
- Jiangsu Key Laboratory of Precious Metals Chemistry and Engineering, School of Chemistry and Environment Engineering
- College of Chemistry and Pharmcy Engineering
- Issue: Vol 40, No 4 (2018)
- Pages: 254-258
- Section: Production, Structure, Properties
- URL: https://journals.rcsi.science/1063-4576/article/view/186257
- DOI: https://doi.org/10.3103/S1063457618040044
- ID: 186257
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Abstract
A solid-state route was developed to prepare zirconium diboride nanosheets with the dimension of about 500 nm and thickness of about 20 nm from zirconium dioxide, iodine and sodium borohydride at 700°C in an autoclave reactor. The obtained ZrB2 product was investigated by X-ray diffraction, scanning electron microscope and transmission electron microscopy. The obtained product was also studied by thermogravimetric analysis. It had good thermal stability and oxidation resistance below 400°C in air. Furthermore, the possible formation mechanism of ZrB2 was also discussed.
About the authors
Liangbiao Wang
Jiangsu Key Laboratory of Precious Metals Chemistry and Engineering, School of Chemistry and Environment Engineering
Author for correspondence.
Email: lbwang@jsut.edu.cn
China, Changzhou, 213001
Dejian Zhao
Jiangsu Key Laboratory of Precious Metals Chemistry and Engineering, School of Chemistry and Environment Engineering
Email: lbwang@jsut.edu.cn
China, Changzhou, 213001
Qinglin Cheng
Jiangsu Key Laboratory of Precious Metals Chemistry and Engineering, School of Chemistry and Environment Engineering
Email: lbwang@jsut.edu.cn
China, Changzhou, 213001
Quanquan Lu
Jiangsu Key Laboratory of Precious Metals Chemistry and Engineering, School of Chemistry and Environment Engineering
Email: lbwang@jsut.edu.cn
China, Changzhou, 213001
Weiqiao Liu
Jiangsu Key Laboratory of Precious Metals Chemistry and Engineering, School of Chemistry and Environment Engineering
Email: lbwang@jsut.edu.cn
China, Changzhou, 213001
Keyan Bao
College of Chemistry and Pharmcy Engineering
Email: lbwang@jsut.edu.cn
China, Nanyang, Henan, 473061
Binglong Zhu
Jiangsu Key Laboratory of Precious Metals Chemistry and Engineering, School of Chemistry and Environment Engineering
Email: lbwang@jsut.edu.cn
China, Changzhou, 213001
Quanfa Zhou
Jiangsu Key Laboratory of Precious Metals Chemistry and Engineering, School of Chemistry and Environment Engineering
Email: lbwang@jsut.edu.cn
China, Changzhou, 213001
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