Spark plasma sintering of β-SiAlON–BN composites from combustion-synthesized powders


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Abstract

Investigated was the spark plasma sintering (SPS) of β-SiAlON/0–30 wt % BN ceramic composites. The raw materials (β-Si5AlON7 and BN powders) were prepared by infiltration-mediated combustion synthesis (CS). Experimentally established were the following process parameters for SPS of composites with high relative density (>95%) and flexural strength of 250–300 MPa: (a) heating rate 50 deg/min, (b) maximum temperature 1650–1750°C, (c) and holding time 5 min.

About the authors

E. V. Nefedova

National Research Nuclear University MEPhI

Email: kosm@ism.ac.ru
Russian Federation, Moscow, 115409

E. G. Grigoryev

National Research Nuclear University MEPhI

Email: kosm@ism.ac.ru
Russian Federation, Moscow, 115409

D. A. Fokin

National Research Nuclear University MEPhI

Email: kosm@ism.ac.ru
Russian Federation, Moscow, 115409

K. L. Smirnov

Institute of Structural Macrokinetics and Materials Science

Author for correspondence.
Email: kosm@ism.ac.ru
Russian Federation, Chernogolovka, Moscow, 142432

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