Fine Ti Powders Through Metallothermic Reduction in TiO2–Mg–Ca Mixtures


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Abstract

Fine Ti powders were prepared through magnesiothermic reduction in TiO2–Mg–Ca mixtures under 4 MPa of Ar followed by acid leaching (with HCl or HNO3) and characterized by XRD, SEM/EDS, and chemical analysis. Thus prepared Ti powders exhibited the specific surface ranging between 7.0 and 30.0 m2/g. The produced Ti powders can find their application in pyrotechnics, powder metallurgy, and as raw material for SHS of inorganic compounds.

About the authors

T. I. Ignat’eva

Institute of Structural Macrokinetics and Materials Science

Email: vervi@ism.ac.ru
Russian Federation, Chernogolovka, Moscow, 142432

V. V. Aleshin

Institute for Problems in Chemical Physics

Email: vervi@ism.ac.ru
Russian Federation, Chernogolovka, Moscow, 142432

Yu. M. Mikhailov

Institute for Problems in Chemical Physics

Email: vervi@ism.ac.ru
Russian Federation, Chernogolovka, Moscow, 142432

V. I. Vershinnikov

Institute of Structural Macrokinetics and Materials Science

Author for correspondence.
Email: vervi@ism.ac.ru
Russian Federation, Chernogolovka, Moscow, 142432

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