Ceramics of the Cs2O–Al2O3 System Prepared by Solid-Phase Technology and the Glycine–Nitrate Combustion Process

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Cs2O–Al2O3 ceramic samples containing 20 and 33 mol % cesium oxide were prepared by сeramic technique and by the glycine–nitrate combustion process. The prepared samples were identified and characterized by X-ray powder diffraction and X-ray fluorescence analyses, scanning electron microscopy, and differential thermal analysis. X-ray powder diffraction and scanning electron microscopy showed that the phase composition and surface of the samples change significantly and nonmonotonically depending on the synthetic method used and the heat treatment parameters of the batch. Optimal synthetic conditions and heat treatment parameters for preparing Cs2O–Al2O3 samples were elucidated.

作者简介

A. Fedorova

St. Petersburg State University

Email: avfiodorova@gmail.com
199034, St. Petersburg, Russia

V. Stolyarov

St. Petersburg State University

Email: avfiodorova@gmail.com
199034, St. Petersburg, Russia

M. Pavelina

St. Petersburg State University

Email: avfiodorova@gmail.com
199034, St. Petersburg, Russia

P. Kolonitskii

St. Petersburg State University

Email: avfiodorova@gmail.com
199034, St. Petersburg, Russia

S. Kirichenko

St. Petersburg State University

Email: avfiodorova@gmail.com
199034, St. Petersburg, Russia

A. Timchuk

St. Petersburg State Electrotechnical University “LETI” named after V.I. Ul’yanov (Lenin)

Email: avfiodorova@gmail.com
197022, St. Petersburg, Russia

V. Stolyarova

St. Petersburg State University

编辑信件的主要联系方式.
Email: avfiodorova@gmail.com
199034, St. Petersburg, Russia

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版权所有 © А.В. Федорова, В.А. Столяров, М.Е. Павелина, П.Д. Колоницкий, С.О. Кириченко, А.В. Тимчук, В.Л. Столярова, 2023

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