Isolation of Concentrated Fractions of Components from Solutions in a Cascade of Multistage Extraction Columns by Recycling Liquid–Liquid Chromatography

A. E. Kostanyan; Костанян А. Е.; Yu. V. Tsareva; Царева Ю. В.; V. V. Belova; Белова В. В.

doi:10.31857/S0044457X22601468

Isolation of Concentrated Fractions of Components from Solutions in a Cascade of Multistage Extraction Columns by Recycling Liquid–Liquid Chromatography

Authors: Kostanyan A.E.¹, Tsareva Y.V.¹, Belova V.V.¹
Affiliations:
1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences
Issue: Vol 68, No 3 (2023)
Pages: 357-362
Section: ФИЗИКОХИМИЯ РАСТВОРОВ
URL: https://journals.rcsi.science/0044-457X/article/view/136337
DOI: https://doi.org/10.31857/S0044457X22601468
EDN: https://elibrary.ru/JDFBZF
ID: 136337

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Abstract
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Abstract

The paper describes the results of an experimental study of the extraction isolation of concentrated fractions of components from solutions by recycling liquid–liquid chromatography in a setup composed of five multistage extraction columns connected in series. The process includes multiple injection of the solution of the components into the system. The adequacy of the previously developed mathematical model to the real process is confirmed and the validity of the obtained equations for the modeling and development of various types of separation processes is demonstrated.

Keywords

liquid extraction, recycling liquid–liquid chromatography, isolation of concentrated fractions of components from solutions

References

Ito Y. // J. Chromatogr. A. 2005. V. 1065. P. 145. https://doi.org/10.1016/j.chroma.2004.12.044
Conway W.D. // J. Chromatogr. A. 2011. V. 1218. P. 6015. https://doi.org/10.1016/j.chroma.2011.03.056
Friesen J.B., Ahmed S., Pauli G.F. // J. Chromatogr. A. 2015. V. 1377. P. 55. https://doi.org/10.1016/j.chroma.2014.11.085
Friesen J.B., McAlpine J.B., Chen S.-N., Pauli G.F. // J. Nat. Prod. 2015. V. 78. P. 1765. https://doi.org/10.1021/np501065h
Huang X.-Y., Pei D., Liu J.-F., Di D.-L. // J. Chromatogr. A. 2018. V. 1531. P. 1. https://doi.org/10.1016/j.chroma.2017.10.073
Li H., Zhang F., Jin Q., Zhu T. // J. Chromatogr. A. 2021. V. 1649. P. 462221. https://doi.org/10.1016/j.chroma.2021.462221
Guilois-Dubois S., Guyot S., Poupard P. // J. Chromatogr. A. 2021. V. 1653. P. 462382. https://doi.org//10.1016/j.chroma.2021.462382
He J.M., Huang J., Wu W.L., Mu Q. // J. Chromatogr. A. 2020. V. 1626. P. 461 368. https://doi.org//10.1016/j.chroma.2020.461368
Yuan Y., He X., Wang T. et al. // Mar. Drugs. 2020. V. 18. P. 332. https://doi.org/10.3390/md18060332
Jerz G., Winterhalter P. // J. Chromatogr. A. 2020. V. 1617. P. 460698. https://doi.org/10.1016/j.chroma.2019.460698
Morley R., Minceva M. // J. Chromatogr. A. 2020. V. 1617. P. 460479. https://doi.org/10.1016/j.chroma.2019.460698
Roehrer S., Minceva M. // Separations. 2019. V. 6. P. 36. https://doi.org/10.3390/separations6030036
Wang C., Sun W., Wang X. et al. // J. Chromatogr. A. 2019. V. 1601. P. 266. https://doi.org/10.1016/j.chroma.2019.05.028
Peng A., Hewitson P., Sutherland I. et al. // J. Chromatogr. A. 2018. V. 1580. P. 120. https://doi.org/10.1016/j.chroma.2018.10.012
Friesen J.B., McAlpine J.B., Chen S.-N., Pauli G.F. // J. Chromatogr. A. 2017. V. 1520. P. 1. https://doi.org/10.1016/j.chroma.2017.08.077
Ignatova S., Sutherland I. // J. Chromatogr. A. 2015. V. 1425. P. 1. https://doi.org/10.1016/j.chroma.2015.10.096
Guan Y.H., Hewitson P., van den Heuvel R. et al. // J. Chromatogr. A. 2015. V. 1424. P. 102. https://doi.org/10.1016/j.chroma.2015.03.004
Ma T., Dong H., Lu H. et al. // J. Chromatogr. A. 2018. V. 1578. P. 61. https://doi.org/10.1016/j.chroma.2018.10.014
Jing J.-X., Muhire J., Sun X. et al. // J. Chromatogr. A. 2022. V. 1677. P. 463319. https://doi.org/10.1016/j.chroma.2022.463319
Müller M., Wasmer K., Vetter W. // J. Chromatogr. A. 2018. V. 1556. P. 88. https://doi.org/10.1016/j.chroma.2018.04.069
Goll J., Minceva M. // AIChE J. 2017. V. 63. P. 1659. https://doi.org/10.1002/AIC.15529
Han Q.B., Song J.Z., Qiao C.F. et al. // J. Chromatogr. A. 2006. V. 1127. P. 298. https://doi.org/10.1016/j.chroma.2006.07.044
Xie J., Deng J., Tan F., Su J. // J. Chromatogr. B. 2010. V. 878878. P. 2665. https://doi.org/10.1016/j.jchromb.2010.07.023
Meng J., Yang Z., Liang J. et al. // J. Chromatogr. A. 2014. V. 1327. P. 27. https://doi.org/10.1016/j.chroma.2013.12.069
Tong S., Guan Y.-X., Yan J. et al. // J. Chromatogr. A. 2011. V. 1218. P. 5434. https://doi.org/10.1016/j.chroma.2011.06.015
Костанян А.Е. // Журн. неорган. химии. 2017. Т. 62. № 12. С. 1666.
Галиева Ж.Н., Семенов А.А., Костанян А.Е., Алдушкин А.В. // Хим. технология. 2020. Т. 21. № 12. C. 565.
Костанян А.Е., Царева Ю.В., Белова В.В., Телешова М.А. // Хим. технология. 2021. Т. 22. № 7. С. 330.
Kostanyan A., Martynova M., Erastov A., Belova V. // J. Chromatogr. A. 2018. V. 1560. P. 26. https://doi.org/10.1016/j.chroma.2018.05.032
Костанян А.Е., Царева Ю.В. // Хим. технология. 2022. Т. 23. № 11.
Kocтaнян A.E., Martynova M. // J. Chromatogr. A. 2020. V. 1614. P. 460735. https://doi.org/10.1016/j.chroma.2019.460735