Аналитические возможности определения углеводов хроматографическими и электрофоретическими методами
- Авторы: Карцова Л.А.1, Малюшевская А.В.1, Колобова Е.А.1,2
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Учреждения:
- Санкт-Петербургский государственный университет
- Всероссийский центр экстренной и радиационной медицины им. А.М. Никифорова МЧС России
- Выпуск: Том 78, № 2 (2023)
- Страницы: 108-128
- Раздел: Обзоры
- URL: https://journals.rcsi.science/0044-4502/article/view/135995
- DOI: https://doi.org/10.31857/S0044450223020044
- EDN: https://elibrary.ru/CDPKAH
- ID: 135995
Цитировать
Аннотация
В обзоре обсуждаются достоинства и ограничения хроматографических и электрофоретических подходов при определении нейтральных углеводов в различных объектах со сложной матрицей, возможность реализации многообразия режимов жидкостной хроматографии и капиллярного электрофореза (в зонном и мицеллярном вариантах), особенности их сочетания с различными вариантами дериватизации, детектирования и пробоподготовки. Обсуждаются условия косвенного детектирования сахаров при введении в подвижную фазу или фоновый электролит различных поглощающих добавок, лигандообменного капиллярного электрофореза и внутрикапиллярного комплексообразования, определение углеводов методами анионообменной и гидрофильной хроматографии.
Об авторах
Л. А. Карцова
Санкт-Петербургский государственный университет
Email: malushevskaa@gmail.com
Россия, 198504, Петродворец, Санкт-Петербург, Университетский просп., 26
А. В. Малюшевская
Санкт-Петербургский государственный университет
Email: malushevskaa@gmail.com
Россия, 198504, Петродворец, Санкт-Петербург, Университетский просп., 26
Е. А. Колобова
Санкт-Петербургский государственный университет; Всероссийский центр экстренной и радиационной медицины им. А.М. Никифорова МЧС России
Автор, ответственный за переписку.
Email: malushevskaa@gmail.com
Россия, 198504, Петродворец, Санкт-Петербург, Университетский просп., 26; Россия, 194044, Санкт-Петербург, ул. Академика Лебедева, 4/2
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