Effect of Pulsed Nitrogen Plasma and Nitrogen Ion Fluxes on the Structure and Mechanical Properties of Vanadium
- 作者: Borovitskaya I.1, Nikulin V.2, Bondarenko G.3, Mikhailova A.1, Silin P.2, Gaidar A.4, Paramonova V.1, Peregudova E.2
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隶属关系:
- Baikov Institute of Metallurgy and Materials Science
- Lebedev Physical Institute (LPI)
- Higher School of Economics
- Research Institute of Advanced Materials and Technologies
- 期: 卷 2018, 编号 3 (2018)
- 页面: 266-275
- 栏目: Article
- URL: https://journals.rcsi.science/0036-0295/article/view/172425
- DOI: https://doi.org/10.1134/S0036029518030023
- ID: 172425
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详细
The effect of powerful pulsed fluxes of nitrogen plasma and nitrogen ions generated in the PF-4 Plasma Focus setup (LPI; energy flux density of plasma pulse was 108–1010 W/cm2) on the modification of vanadium surface is studied. Melting and ultrafast solidification result in a fine cellular structure (cell size of 100–200 nm) in a thin surface layer in samples. There are irradiation regimes causing directional crack growth after solidification and cooling of the surface layer and the formation of a block microstructure with a block size of several tens of micrometers. The thickness of the melted layer in the samples is 2–4 μm. Cracks propagate to a depth of 5–20 μm. It is established that irradiation by pulsed nitrogen plasma and high-energy nitrogen ions changes the microhardness of the vanadium surface layers. The microhardness increases by a factor of three with the number of plasma pulses and the distance between a sample and the anode of the Plasma Focus (PF) setup. The increase in the microhardness is in agreement with the refinement of coherent scattering regions, the increase in lattice microstrain ε, and the formation of vanadium nitrides. Pulsed fluxes of nitrogen plasma and nitrogen ions decrease the lattice parameter much greater than cold working (rolling) does. The lattice parameter decreases when the total irradiation power is increased (the number of pulses increases or the distance between a sample and the anode of the PF setup decreases). Such changes seem to be caused by the action of the residual macrostresses induced by pulsed plasma irradiation. In addition, X-ray diffraction analysis showed a change in the texture of the surface layer after ion-plasma treatment of coldworked vanadium samples in the PF setup.
作者简介
I. Borovitskaya
Baikov Institute of Metallurgy and Materials Science
编辑信件的主要联系方式.
Email: symp@imet.ac.ru
俄罗斯联邦, Moscow, 119334
V. Nikulin
Lebedev Physical Institute (LPI)
Email: symp@imet.ac.ru
俄罗斯联邦, Moscow, 119991
G. Bondarenko
Higher School of Economics
Email: symp@imet.ac.ru
俄罗斯联邦, Moscow, 101000
A. Mikhailova
Baikov Institute of Metallurgy and Materials Science
Email: symp@imet.ac.ru
俄罗斯联邦, Moscow, 119334
P. Silin
Lebedev Physical Institute (LPI)
Email: symp@imet.ac.ru
俄罗斯联邦, Moscow, 119991
A. Gaidar
Research Institute of Advanced Materials and Technologies
Email: symp@imet.ac.ru
俄罗斯联邦, Moscow, 115054
V. Paramonova
Baikov Institute of Metallurgy and Materials Science
Email: symp@imet.ac.ru
俄罗斯联邦, Moscow, 119334
E. Peregudova
Lebedev Physical Institute (LPI)
Email: symp@imet.ac.ru
俄罗斯联邦, Moscow, 119991
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