Nickel Itaconate Thermolysis


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Abstract

Experimental-statistical mathematical models are built for nickel itaconate thermolysis to relate some response functions (carbon, hydrogen, oxygen, and nickel concentrations in the nanocomposite, yield of the nanocomposite, contents of β-nickel and nickel oxide phases, and nanoparticle diameter) to the thermolysis temperature and time. Response surfaces are constructed to illustrate the dependence of the above-listed response functions on the thermolysis temperature and time. These response functions are analyzed to determine the synthetic parameters that would provide the preparation of nanocomposites with tailored characteristics, in particular, with the highest content of the magnetoactive β-nickel phase.

About the authors

S. A. Semenov

MIREA—Russian Technological University (Lomonosov Institute of Fine Chemical Technologies)

Author for correspondence.
Email: srg.semenov@gmail.com
Russian Federation, Moscow, 119454

V. Yu. Musatova

MIREA—Russian Technological University (Lomonosov Institute of Fine Chemical Technologies)

Email: srg.semenov@gmail.com
Russian Federation, Moscow, 119454

D. V. Drobot

MIREA—Russian Technological University (Lomonosov Institute of Fine Chemical Technologies)

Email: srg.semenov@gmail.com
Russian Federation, Moscow, 119454

G. I. Dzhardimalieva

Institute of Problems of Chemical Physics

Email: srg.semenov@gmail.com
Russian Federation, Chernogolovka, Moscow oblast, 142432

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