The structure of the cobalt metal particles formed in Co3O4 reduction microspheres produced by ultrasonic spray pyrolysis


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Abstract

The process of the reduction spherical Co3O4 particles to metallic Co in a continuous H2 flow at the temperature interval (200–350°C) was studied using the XRD method. The phase analysis of the reduced particles showed their non-single state (the coexistence of α-Co and β-Co). The β-Co concentration increases with an increase in the reduction temperature.

About the authors

A. A. Novakova

Faculty of Physics

Author for correspondence.
Email: novakova.alla@gmail.com
Russian Federation, Moscow, 119991

A. V. Dolzhikova

Faculty of Physics

Email: novakova.alla@gmail.com
Russian Federation, Moscow, 119991

N. V. Shatrova

MISiS National University of Science and Technology

Email: novakova.alla@gmail.com
Russian Federation, Moscow, 119049

V. V. Levina

MISiS National University of Science and Technology

Email: novakova.alla@gmail.com
Russian Federation, Moscow, 119049

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