Application of microemulsions for the extraction of o-phthalate esters from soil with subsequent separation of microemulsions, simultaneous preconcentration, and gas chromatographic analysis of target components
- Authors: Tolmacheva N.G.1, Pirogov A.V.1, Shpigun O.A.1
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Affiliations:
- Chemistry Department
- Issue: Vol 72, No 2 (2017)
- Pages: 92-96
- Section: Article
- URL: https://journals.rcsi.science/0027-1314/article/view/163418
- DOI: https://doi.org/10.3103/S0027131417020043
- ID: 163418
Cite item
Abstract
The possible application of microemulsions as extractants for the extraction of o-phthalate esters from soils with the subsequent breakdown of microemulsions, simultaneous preconcentration of dialkhylphthalates in the organic phase, and their following gas chromatographic analysis with mass-spectrometric detection is demonstrated. The preconcentration factor was 18. The method is characterized by low detection limits, good selectivity, and reproducibility.
About the authors
N. G. Tolmacheva
Chemistry Department
Author for correspondence.
Email: tolmacheva-natali@mail.ru
Russian Federation, Moscow
A. V. Pirogov
Chemistry Department
Email: tolmacheva-natali@mail.ru
Russian Federation, Moscow
O. A. Shpigun
Chemistry Department
Email: tolmacheva-natali@mail.ru
Russian Federation, Moscow
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