DETERMINATION OF THE ABSOLUTE CONFIGURATION OF MONOATOMIC CHIRAL CRYSTALS USING THREE-WAVE X-RAY DIFFRACTION

K. A. Kozlovskaya; Козловская К. А.; E. N. Ovchinnikova; Овчинникова Е. Н.; A. M. Ustyugov; Устюгов А. М.; V. E. Dmitrienko; Дмитриенко В. Е.; A. P. Oreshko; Орешко А. П.

doi:10.31857/S0023476123700066

DETERMINATION OF THE ABSOLUTE CONFIGURATION OF MONOATOMIC CHIRAL CRYSTALS USING THREE-WAVE X-RAY DIFFRACTION

Autores: Kozlovskaya K.¹, Ovchinnikova E.¹, Ustyugov A.¹, Dmitrienko V.², Oreshko A.¹
Afiliações:
1. Lomonosov Moscow State University, Moscow, 119991 Russia
2. Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,” Russian Academy of Sciences, Moscow, 119333 Russia
Edição: Volume 68, Nº 3 (2023)
Páginas: 370-375
Seção: ДИФРАКЦИЯ И РАССЕЯНИЕ ИОНИЗИРУЮЩИХ ИЗЛУЧЕНИЙ
URL: https://journals.rcsi.science/0023-4761/article/view/137400
DOI: https://doi.org/10.31857/S0023476123700066
EDN: https://elibrary.ru/WZXZDW
ID: 137400

Citar

Texto integral

Acesso aberto
Acesso é fechado

Acesso está concedido
Acesso é fechado

Somente assinantes

Resumo
Sobre autores
Bibliografia
Arquivos suplementares
Estatísticas

Resumo

Many molecules and crystals are chiral, i.e., can exist as right- and left-handed mirror isomers. It is shown that the absolute configuration of monoatomic chiral crystals, including selenium, tellurium, and b-manganese, can be determined using multi-wavelength diffraction of circularly polarized X-ray radiation.

Palavras-chave

ABSOLUTE CONFIGURATION, CHIRAL CRYSTALS, THREE-WAVE X-RAY DIFFRACTION

Sobre autores

K. Kozlovskaya

Lomonosov Moscow State University, Moscow, 119991 Russia

Email: kozlovskaya@physics.msu.ru
Россия, Москва

E. Ovchinnikova

Lomonosov Moscow State University, Moscow, 119991 Russia

Email: ovtchin@gmail.com
Россия, Москва

A. Ustyugov

Lomonosov Moscow State University, Moscow, 119991 Russia

Email: kozlovskaya@physics.msu.ru
Россия, Москва

V. Dmitrienko

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,” Russian Academy of Sciences, Moscow, 119333 Russia

Email: ovtchin@gmail.com
Россия, Москва

A. Oreshko

Lomonosov Moscow State University, Moscow, 119991 Russia

Autor responsável pela correspondência
Email: ap.oreshko@physics.msu.ru
Россия, Москва

Bibliografia

Nguyen L.A., He H., Pham-Huy C. // Int. J. Biomed. Sci. 2006. V. 2. № 2. P. 85.
Yang S.H. // Nat. Mater. 2022. V. 21. № 5. P. 494. https://doi.org/10.1038/s41563-022-01228-y
Calavalle F., Suárez-Rodríguez M., Martín-García B. et al. // Nat. Mater. 2022. V. 21. № 5. P. 526. https://doi.org/10.1038/s41563-022-01211-7
McIntyre G.J. // Acta Cryst. 1978. V. 34. P. 936. https://doi.org/10.1107/S0567739478001916
Brown P.J., Forsyth J.B. // Acta Cryst. A. 1996. V. 52. № 3. P. 408. https://doi.org/10.1107/S0108767395017144
Tanaka Y., Kojima T., Takata Y. et al. // Phys. Rev. B. 2010. V. 81. № 14. P. 144104. https://doi.org/10.1103/PhysRevB.81.144104
Winkelmann A., Cios G., Tokarski T. et al. // arXiv:2011.14422v1. 2020. V. 1. P. 1.
Renninger M. // Z. Phys. 1937. B. 106. № 3–4. S. 141. https://doi.org/10.1007/BF01340315
Kozlovskaya K., Ovchinnikova E., Kokubun J. et al. // Crystals. 2021. V. 11. № 11. P. 1389. https://doi.org/10.3390/cryst11111389
Mayer G. // Z. Krist. 1928. B. 66. № 1. S. 585. https://doi.org/10.1524/zkri.1928.66.1.585
Authier A. // International Tables for Crystallography. Dordrecht: Springer, 2006. V. B. P. 534. https://doi.org/10.1107/97809553602060000569
Kokubun J., Ishida K., Dmitrienko V.E. // J. Phys. Soc. Jpn. 1998. V. 67. № 4. P. 1291. https://doi.org/10.1143/jpsj.67.1291
Kokubun J., Kanazawa M., Ishida K., Dmitrienko V.E. // Phys. Rev. B. 2001. V. 64. № 7. P. 073203. https://doi.org/10.1103/PhysRevB.64.073203
Дмитриенко В.Е., Овчинникова Е.Н. // Кристаллография. 2003. Т. 48. № 6. С. S59.
Козловская К.А., Устюгов А., Иванов С.В. и др. // Ученые записки физического факультета московского университета. 2020. Т. 6. С. 1.
Kozlovskaya K.A., Kulikov A.G., Novikov D. et al. // Cryst. Res. Technol. 2021. V. 56. P. 2000195. https://doi.org/10.1002/crat.202000195
Ovchinnikova E., Novikov D., Zschornak M. et al. // Crystals. 2020. V. 10. № 9. P. 719. https://doi.org/10.3390/cryst10090719
Ovchinnikova E.N., Rogalev A., Wilhelm F. et al. // J. Synchrotron Radiat. 2021. V. 28. P. 1455. https://doi.org/10.1107/S1600577521005853
Rogalev A., Wilhelm F., Ovchinnikova E. et al. // Crystals. 2021. V. 11. P. 544. https://doi.org/10.3390/cryst11050544
Preston G.D. // London, Edinburgh, Dublin Philos. Mag. J. Sci. 1928. V. 5. № 33. P. 1207. https://doi.org/10.1080/14786440608564570
Засимов В.С., Кузьмин Р.Н., Александров А.Ю. и др. // Письма в ЖЭТФ. 1972. Т. 15. № 7. С. 394.
Avilov A.S., Imamov R.M. // Soviet Physics Crystallography. 1969. V. 14. P. 259.
Bradley A.J. // London, Edinburgh, Dublin Philos. Mag. J. Sci. 1924. V. 48. № 285. P. 477. https://doi.org/10.1080/14786442408634511
Платунов М.С., Зубавичус Я.В., Овчинников С.Г. и др. // Технологическая инфраструктура сибирского кольцевого источника фотонов “СКИФˮ. Новосибирск: ФИЦ “Институт катализа им. Г.К. Борескова СО РАНˮ, 2022. Т. 3. С. 313.