Crystal Structure of Na 2 [OsCl 6 ]

O. V. Rudnitskaya; E. K. Kultyshkina; E. V. Dobrokhotova; T. A. Tereshina; A. S. Popova; Ya. V. Zubavichus; V. N. Khrustalev

doi:10.1134/S0022476619070096

Crystal Structure of Na₂[OsCl₆]

Authors: Rudnitskaya O.V.¹, Kultyshkina E.K.¹, Dobrokhotova E.V.¹, Tereshina T.A.¹, Popova A.S.¹, Zubavichus Y.V.², Khrustalev V.N.¹
Affiliations:
1. People’s Friendship University of Russia
2. Boreskov Institute of Catalysis, Siberian Branch
Issue: Vol 60, No 7 (2019)
Pages: 1086-1090
Section: Article
URL: https://journals.rcsi.science/0022-4766/article/view/162148
DOI: https://doi.org/10.1134/S0022476619070096
ID: 162148

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Abstract

Salt Na₂[OsCl₆] is obtained by the interaction of H₂[OsCl₆]·H₂O with NaCl in boiling concentrated hydrochloric acid. According to the single crystal X-ray diffraction data, the substance crystallizes in the cubic system, space group Fm3̄m, a = 9.7461(11) Å, V= 925.8(3) Å³, Z = 4, R₁= 0.029, wR₂ = 0.070. The compound is characterized by UV-vis and IR spectroscopy.