Structure and magnetic properties of pure and samarium doped magnetite nanoparticles
- Авторы: Polozhentsev O.E.1, Kubrin S.P.2, Butova V.V.1, Kochkina V.K.1, Soldatov A.V.1, Stashenko V.V.2
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Учреждения:
- Southern Federal University
- Research Institute of Physics
- Выпуск: Том 57, № 7 (2016)
- Страницы: 1459-1468
- Раздел: Applications of Synchrotron Radiation in Structural Chemistry
- URL: https://journals.rcsi.science/0022-4766/article/view/160689
- DOI: https://doi.org/10.1134/S0022476616070222
- ID: 160689
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Аннотация
In this paper, a study of pure and doped samarium magnetite nanoparticles synthesized using a microwave synthesis in aqueous solution was performed. The shape, size and structure of the pure and samarium doped magnetite nanoparticles were determined by X-ray diffraction, transmission electron microscopy, X-ray absorption spectroscopy and Mössbauer spectroscopy. The magnetic properties of the nanoparticles were investigated using a vibrating sample magnetometer. It was found that the samarium doped magnetite nanoparticles were superparamagnetic with high saturation magnetization. The doping with a small amount of samarium allowed to reduce the size of nanoparticles, their size distribution, increase resistance to oxidation and improve their magnetic characteristics.
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O. Polozhentsev
Southern Federal University
Автор, ответственный за переписку.
Email: olegpolozhentsev@mail.ru
Россия, Rostov-on-Don
S. Kubrin
Research Institute of Physics
Email: olegpolozhentsev@mail.ru
Россия, Rostov-on-Don
V. Butova
Southern Federal University
Email: olegpolozhentsev@mail.ru
Россия, Rostov-on-Don
V. Kochkina
Southern Federal University
Email: olegpolozhentsev@mail.ru
Россия, Rostov-on-Don
A. Soldatov
Southern Federal University
Email: olegpolozhentsev@mail.ru
Россия, Rostov-on-Don
V. Stashenko
Research Institute of Physics
Email: olegpolozhentsev@mail.ru
Россия, Rostov-on-Don
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