A New Method of Synthesis of Nanosized Boehmite (AlOOH) Powders with a Low Impurity Content


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Abstract

A new method of synthesis of nanosized aluminum oxyhydroxide (AlOOH, boehmite) powders has been suggested through a hydrothermal treatment of nanosized γ-Al2O3 powder in water and a 1.5 wt % HCl solution at different temperatures. It has been found that hydrothermal treatment in a 1.5 wt % HCl solution leads to the purification of the starting material; different treatment durations allow one to obtain boehmite particles of different shape. It has been demonstrated that a nanosized boehmite powder is obtained upon the hydrothermal treatment of a nanosized γ-Al2O3 in water above 80°С. The nanosized boehmite powders synthesized at different temperatures have been studied by various methods.

About the authors

G. N. Panasyuk

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Author for correspondence.
Email: panasyk@igic.ras.ru
Russian Federation, Moscow, 119991

E. A. Semenov

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: irina135714@yandex.ru
Russian Federation, Moscow, 119991

I. V. Kozerozhets

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Author for correspondence.
Email: irina135714@yandex.ru
Russian Federation, Moscow, 119991

L. A. Azarova

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: irina135714@yandex.ru
Russian Federation, Moscow, 119991

V. N. Belan

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: irina135714@yandex.ru
Russian Federation, Moscow, 119991

M. N. Danchevskaya

Moscow State University

Email: irina135714@yandex.ru
Russian Federation, Moscow, 119991

G. E. Nikifirova

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: irina135714@yandex.ru
Russian Federation, Moscow, 119991

I. L. Voroshilov

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: irina135714@yandex.ru
Russian Federation, Moscow, 119991

S. A. Pershikov

Moscow Polytechnic University

Email: irina135714@yandex.ru
Russian Federation, Moscow, 107023

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