Synthesis of Prolylproline

V. A. Gaidukevich; L. A. Popova; Z. P. Zubreichuk; V. A. Knizhnikov

doi:10.1134/S1070428019070169

Synthesis of Prolylproline

作者: Gaidukevich V.A.¹, Popova L.A.¹, Zubreichuk Z.P.¹, Knizhnikov V.A.¹
隶属关系:
1. Institute of Physical Organic Chemistry
期: 卷 55, 编号 7 (2019)
页面: 1005-1008
栏目: Article
URL: https://journals.rcsi.science/1070-4280/article/view/220918
DOI: https://doi.org/10.1134/S1070428019070169
ID: 220918

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Prolylproline has been synthesized by both classical peptide synthesis method utilizing tert-butoxycarbonyl or trifluoroacetyl protection of the NH group and carbodiimide-promoted peptide bond formation and by opening of the dioxopiperazine ring in octahydrodipyrrolo[1,2-a:1′,2′-d]pyrazine-5,10-dione obtained by thermolysis of proline methyl ester.