Study of the K2Ni(SO4)2 ∙ 6H2O–K2Co(SO4)2 ∙ 6H2O–H2O diagram and determination of the conditions for growing K2(Ni,Co)(SO4)2 ∙ 6H2O mixed crystals


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The phase diagram of the K2Ni(SO4)2 · 6H2O–K2Co(SO4)2 · 6H2O–H2O ternary system is investigated in the temperature range of 30–70°С, and a relationship between the compositions of the equilibrium phases of the K2CoxNi(1–x)(SO4)2 · 6H2O (KCNSH) solid solution and the growth solution is established. It is shown how the salt compositions of the liquid and solid phases change during crystal growth upon slow cooling of solution. A dependence of the lattice parameters of the KCNSH solid solution on the concentration of isomorphic components is experimentally found.

作者简介

A. Zhokhov

Institute of Solid State Physics

Email: emelch@issp.ac.ru
俄罗斯联邦, Chernogolovka, 142432

V. Masalov

Institute of Solid State Physics

Email: emelch@issp.ac.ru
俄罗斯联邦, Chernogolovka, 142432

I. Zverkova

Institute of Solid State Physics

Email: emelch@issp.ac.ru
俄罗斯联邦, Chernogolovka, 142432

G. Emelchenko

Institute of Solid State Physics

编辑信件的主要联系方式.
Email: emelch@issp.ac.ru
俄罗斯联邦, Chernogolovka, 142432

V. Manomenova

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”

Email: emelch@issp.ac.ru
俄罗斯联邦, Moscow, 119333

E. Rudneva

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”

Email: emelch@issp.ac.ru
俄罗斯联邦, Moscow, 119333

N. Vasilieva

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”

Email: emelch@issp.ac.ru
俄罗斯联邦, Moscow, 119333

A. Voloshin

Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”

Email: emelch@issp.ac.ru
俄罗斯联邦, Moscow, 119333

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