Crystal Structure of 3-[1-(4-Methylphenyl)-9,10-dihydro-4-azaphenanthren-3-yl]benzo[f]coumarin
- Авторы: Sharma D.1, Sharma N.2, Brahmbhatt D.3, Gupta V.4
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Учреждения:
- Government Boys Higher Secondary School, Akhnoor
- Government Degree College Ramnagar
- Department of Chemistry, Sardar Patel University
- X-ray Crystallography Laboratory, Post-Graduate Department of Physics and Electronics, University of Jammu
- Выпуск: Том 64, № 7 (2019)
- Страницы: 1047-1050
- Раздел: Structure of Organic Compounds
- URL: https://journals.rcsi.science/1063-7745/article/view/194405
- DOI: https://doi.org/10.1134/S1063774519070198
- ID: 194405
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Аннотация
The crystal structure of the title compound is determined by single crystal X-ray structure analysis. The structure was solved by direct method and refined to a final R-value of 0.0469 for 2826 observed reflections. The benzocoumarin ring system is planar. The central ring of 4-azaphenantrene moiety has a half chair conformation, phenyl substituent forms dihedral angle of 56.46° with the mean plane of 4-azaphenantrene system. The coumarin system is rotated relative to the latter by 15.48(2)°. This orientation is stabilized by two weak intramolecular C–H···N hydrogen bonds.
Об авторах
Deepak Sharma
Government Boys Higher Secondary School, Akhnoor
Email: nareshbasotra@gmail.com
Индия, Jammu (J & K)
Naresh Sharma
Government Degree College Ramnagar
Email: nareshbasotra@gmail.com
Индия, Jammu (J & K)
D. Brahmbhatt
Department of Chemistry, Sardar Patel University
Email: nareshbasotra@gmail.com
Индия, Vallabh Vidyanagar, Gujarat
Vivek Gupta
X-ray Crystallography Laboratory, Post-Graduate Department of Physics and Electronics, University of Jammu
Автор, ответственный за переписку.
Email: nareshbasotra@gmail.com
Индия, Jammu Tawi, 180 006