Structure of Cs 4 (HSO 4 ) 3 (H 2 PO 4 ) single crystals

I. P. Makarova; V. V. Grebenev; I. I. Vasil’ev; E. V. Dmitricheva; V. A. Komornikov; V. V. Dolbinina; A. S. Mikheikin

doi:10.1134/S1063774516010119

Structure of Cs₄(HSO₄)₃(H₂PO₄) single crystals

Authors: Makarova I.P.¹, Grebenev V.V.¹, Vasil’ev I.I.¹, Dmitricheva E.V.¹, Komornikov V.A.¹, Dolbinina V.V.¹, Mikheikin A.S.²^,3
Affiliations:
1. Shubnikov Institute of Crystallography
2. Swiss–Norwegian Beamlines
3. Faculty of Physics
Issue: Vol 61, No 1 (2016)
Pages: 18-23
Section: Structure of Inorganic Compounds
URL: https://journals.rcsi.science/1063-7745/article/view/189576
DOI: https://doi.org/10.1134/S1063774516010119
ID: 189576

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Abstract

Single crystals of Cs₄(HSO₄)₃(H₂PO₄) are synthesized and studied for the first time. The new compound is found in the course of studies of the phase diagram of the CsHSO₄–CsH₂PO₄–H₂O triple system. Data on the atomic crystal structure of single-crystalline and powder specimens, as well as on structural phase transitions, are obtained.