Enviar artigo por via de e-mail Rhenium(V) Tris(pyrazolyl)borate Complexes as Ligands in Square Planar Palladium and Platinum Complexes
- Autores: Skabitskii I.V.1, Il’ina Y.Y.1, Shapovalov S.S.1
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Afiliações:
- Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, 119991, Moscow, Russia
- Edição: Volume 49, Nº 1 (2023)
- Páginas: 36-43
- Seção: Articles
- URL: https://journals.rcsi.science/0132-344X/article/view/137263
- DOI: https://doi.org/10.31857/S0132344X22700086
- EDN: https://elibrary.ru/ESDZQX
- ID: 137263
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Resumo
The reactions of TpReO(SnC3H7)2 (Tp = tris(pyrazolyl)borate anion) with acetonitrile complexes PdCl2(MeCN)2 and PtI2(MeCN)2 in toluene solutions resulted in the formation of new heterometallic rhenium complexes TpReO(µ-SnC3H7)2MX2 (MX2 = PdCl2 (I), MX2 = PtI2 (II)). A similar complex TpReO(µ-SnC3H7)2PdI2 (III) was formed either on treatment of I with NaI in dichloromethane or in the reaction of TpReO(SnC3H7)2 with a suspension of PdI2 in toluene. Complexes I–III were characterized by IR and NMR spectroscopy and by X-ray diffraction (CCDC nos. 2172225–2172227).
Sobre autores
I. Skabitskii
Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, 119991, Moscow, Russia
Autor responsável pela correspondência
Email: skabitskiy@gmail.com
Россия, Москва
Yu. Il’ina
Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, 119991, Moscow, Russia
Email: skabitskiy@gmail.com
Россия, Москва
S. Shapovalov
Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, 119991, Moscow, Russia
Email: skabitskiy@gmail.com
Россия, Москва
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