Effect of glass crystallization parameters on conductivity of Li1.5+xAl0.5Ge1.5SixP3–xO12 glass-ceramics
- Autores: Kuznetsova E.1, Pershina S.1, Kuznetsova T.1
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Afiliações:
- Institute of High Temperature Electrochemistry, Ural Branch of the Russian Academy of Sciences
- Edição: Volume 93, Nº 10 (2023)
- Páginas: 1633-1640
- Seção: Articles
- URL: https://journals.rcsi.science/0044-460X/article/view/247203
- DOI: https://doi.org/10.31857/S0044460X23100116
- EDN: https://elibrary.ru/PMUEWK
- ID: 247203
Citar
Resumo
Glass-ceramic samples of the Li1.5+ x Al0.5Ge1.5Si x P3- x O12 system ( x = 0-0.1) were obtained by directional crystallization of glasses. The glass transition, onset and peak temperatures of crystallization were determined using differential scanning calorimetry. The phase composition of glass-ceramics was determined by X-ray phase analysis. Electrical conductivity is studied using electrochemical impedance. Based on the data obtained, the homogeneity region of solid solutions was established and the optimal conditions for producing SiO2-doped glass-ceramics were identified. The composition with x = 0.02, crystallized at 750°C with a heating rate of 3 deg/min for 2 h, had the highest lithium-ion conductivity at room temperature (4.55×10-4 S/cm).
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Sobre autores
E. Kuznetsova
Institute of High Temperature Electrochemistry, Ural Branch of the Russian Academy of Sciences
S. Pershina
Institute of High Temperature Electrochemistry, Ural Branch of the Russian Academy of Sciences
Email: svpershina_86@mail.ru
T. Kuznetsova
Institute of High Temperature Electrochemistry, Ural Branch of the Russian Academy of Sciences
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