Email this article Synthesis and spectral characteristics of hydrazinocarbonothioyl derivatives of maleopimaric acid
- Authors: Vafina G.F1, Poptsov A.I1
-
Affiliations:
- Ufa Institute of Chemistry, Ufa Federal Research Center of the Russian Academy of Sciences
- Issue: Vol 93, No 8 (2023)
- Pages: 1178-1189
- Section: Articles
- URL: https://journals.rcsi.science/0044-460X/article/view/141615
- DOI: https://doi.org/10.31857/S0044460X23080048
- EDN: https://elibrary.ru/IXDICT
- ID: 141615
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Abstract
Reaction of acyl isothiocyanates of 2-allyl- and 2-benzylmaleopimarimides with 3-carboxy- and 2,4-dinitrophenylhydrazines and hydrazides of some aromatic acids (benzoic, 4-hydroxy- and 4-methoxybenzoic, nicotinic, isonicotinic) furnished linear hydrazinocarbonothioyl derivatives of these maleopimarimides in high yields. Structure of the synthesized compounds was determined by 1H,13C, 1H-13C HSQC, 1H-13C HMBC, COSY, NOESY, and 1H-15N HMBC NMR spectroscopy methods.
About the authors
G. F Vafina
Ufa Institute of Chemistry, Ufa Federal Research Center of the Russian Academy of Sciences
Email: vafina@anrb.ru
A. I Poptsov
Ufa Institute of Chemistry, Ufa Federal Research Center of the Russian Academy of Sciences
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