Anion-Exchange Resin Precipitation of Nickel Ferrite Nanopowders Modified by Plasmonic Particles

S. V. Saikova; Сайкова С. В.; D. I. Nemkova; Немкова Д. И.; E. V. Pikurova; Пикурова Е. В.; A. S. Samoilo; Самойло А. С.

doi:10.31857/S0044457X23600160

Anion-Exchange Resin Precipitation of Nickel Ferrite Nanopowders Modified by Plasmonic Particles

Authors: Saikova S.V.¹^,2, Nemkova D.I.², Pikurova E.V.¹^,2, Samoilo A.S.²
Affiliations:
1. Institute of Chemistry and Chemical Engineering, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences
2. Siberian Federal University
Issue: Vol 68, No 8 (2023)
Pages: 1011-1020
Section: СИНТЕЗ И СВОЙСТВА НЕОРГАНИЧЕСКИХ СОЕДИНЕНИЙ
URL: https://journals.rcsi.science/0044-457X/article/view/136395
DOI: https://doi.org/10.31857/S0044457X23600160
EDN: https://elibrary.ru/MKWNNB
ID: 136395

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Abstract
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Abstract

Magnetic nickel ferrite/gold hybrid nanoparticles are promising materials for use in medicine, microelectronics, and plasmon-enhanced photocatalysis. The catalytic activity of a hybrid material depends on the composition, morphology, surface charge, and size of the magnetic core. In this work, anion-exchange resin coprecipitation of iron and nickel followed by heat treatment of the prepared hydroxides was used to manufacture nickel ferrite NiFe2O4 nanopowders. Fractional factorial design (FFD 27-4) was used to study the effects of reaction parameters on NiFe2O4 formation. The synthesis under the found optimal conditions yielded powders with an average grain size of 22.7 ± 1.0 nm. NiFe2O4/Au hybrid particles were manufactured by the direct reduction of gold with methionine (α-amino-γ-methylthiobutyric acid). Their formation was proved by optical spectroscopy, transmission electron microscopy, and X-ray photoelectron spectroscopy.

Keywords

ferrite, anion exchanger, hybrid nanoparticles

References

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